C₃₃H₄₀N₃O₅P

Base Information

Chemical Name:C₃₃H₄₀N₃O₅P
CAS No.:1393821-84-5
Molecular Formula:C₃₃H₄₀N₃O₅P
Molecular Weight:589.671
Hs Code.:

C<sub>33</sub>H<sub>40</sub>N<sub>3</sub>O<sub>5</sub>P

Synonyms:C₃₃H₄₀N₃O₅P

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Chemical Property of C₃₃H₄₀N₃O₅P

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Technology Process of C₃₃H₄₀N₃O₅P

There total 4 articles about C₃₃H₄₀N₃O₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1393821-76-5
azido-L-Leu-L-Phe-OMe

: 1393821-70-9
diphenylphosphine proline phenyl ester

: 1393821-84-5
C₃₃H₄₀N₃O₅P

Guidance literature:: In aq. phosphate buffer; N,N-dimethyl-formamide; at 20 ℃; for 0.5h; pH=7.4;
DOI:10.1021/ol3022484

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1393821-84-5
C₃₃H₄₀N₃O₅P

Guidance literature:: Multi-step reaction with 4 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0.17 h / 20 °C

1.2: 1 h / 20 °C

2.1: ammonium chloride; sulfuric acid / ethyl acetate / 0.5 h / 20 °C

3.1: triethylamine / dichloromethane / 3 h / 0 °C

4.1: N,N-dimethyl-formamide; aq. phosphate buffer / 0.5 h / 20 °C / pH 7.4

With dmap; sulfuric acid; ammonium chloride; triethylamine; dicyclohexyl-carbodiimide; In aq. phosphate buffer; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 4.1: |Staudinger Azide Reduction;
DOI:10.1021/ol3022484

Reference yield:

: L-proline phenyl ester HCl

: 1393821-84-5
C₃₃H₄₀N₃O₅P

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 3 h / 0 °C

2: N,N-dimethyl-formamide; aq. phosphate buffer / 0.5 h / 20 °C / pH 7.4

With triethylamine; In aq. phosphate buffer; dichloromethane; N,N-dimethyl-formamide; 2: |Staudinger Azide Reduction;
DOI:10.1021/ol3022484