C₆₅H₆₀N₂O₄

Base Information

• Chemical Name: C₆₅H₆₀N₂O₄
• CAS No.: 1621070-12-9
• Molecular Formula: C₆₅H₆₀N₂O₄
• Molecular Weight: 933.202
• Mol file: 1621070-12-9.mol

Synonyms:C₆₅H₆₀N₂O₄

Chemical Property of C₆₅H₆₀N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₅H₆₀N₂O₄

There total 6 articles about C₆₅H₆₀N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

N-(4-hydroxyphenyl)formamide (1693-39-6) + C51H48Br2 (1621070-11-8) → C65H60N2O4 (1621070-12-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.dyepig.2014.06.025

Reference yield:

2,7-dibromo-9,9-bis(6-bromohexyl)fluorene (570414-33-4) → C65H60N2O4 (1621070-12-9)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Schlenk technique

2: potassium carbonate / N,N-dimethyl-formamide / 60 °C / Inert atmosphere; Schlenk technique

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;

DOI:10.1016/j.dyepig.2014.06.025

Reference yield:

1 ,6-dibromohexane (629-03-8) → C65H60N2O4 (1621070-12-9)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide; tetrabutylammomium bromide / Inert atmosphere; Schlenk technique

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Schlenk technique

3: potassium carbonate / N,N-dimethyl-formamide / 60 °C / Inert atmosphere; Schlenk technique

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate; potassium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;

DOI:10.1016/j.dyepig.2014.06.025

upstream raw materials:

1 ,6-dibromohexane

2,7-dibromo-9H-fluorene

N-(4-hydroxyphenyl)formamide

C₅₁H₄₈Br₂