carbonic acid, 1-cyano-3-phenylpropyl ethyl ester

Base Information

Chemical Name:carbonic acid, 1-cyano-3-phenylpropyl ethyl ester
CAS No.:1040148-02-4
Molecular Formula:C₁₃H₁₅NO₃
Molecular Weight:233.267
Hs Code.:

Synonyms:carbonic acid, 1-cyano-3-phenylpropyl ethyl ester

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Chemical Property of carbonic acid, 1-cyano-3-phenylpropyl ethyl ester

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Technology Process of carbonic acid, 1-cyano-3-phenylpropyl ethyl ester

There total 2 articles about carbonic acid, 1-cyano-3-phenylpropyl ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 104-53-0
3-phenyl-propionaldehyde

: 623-49-4
ethyl cyanoformate

: 1040148-02-4
carbonic acid, 1-cyano-3-phenylpropyl ethyl ester

Guidance literature:: With 3-(diethylamino)propyltrimethoxysilane supported on silica-alumina; In toluene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.200702048

Reference yield: 61.0%

: 201230-82-2
carbon monoxide

: 103-63-9
1-phenyl-2-bromoethane

: 623-49-4
ethyl cyanoformate

: 1040148-02-4
carbonic acid, 1-cyano-3-phenylpropyl ethyl ester

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃; for 3h; under 91206.1 Torr;
DOI:10.3762/bjoc.10.12

Reference yield: 27.0%

: 4224-69-5
methyl 2-(bromomethyl)propenoate

: 1040148-02-4
carbonic acid, 1-cyano-3-phenylpropyl ethyl ester

: 1373932-53-6
C₁₈H₂₁NO₅

Guidance literature:: carbonic acid, 1-cyano-3-phenylpropyl ethyl ester; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

methyl 2-(bromomethyl)propenoate; In tetrahydrofuran; at -78 ℃;
DOI:10.1021/ol3007716