17β-Hydroxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-3-one 17-Benzoate

Base Information

Chemical Name:17β-Hydroxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-3-one 17-Benzoate
CAS No.:126792-26-5
Molecular Formula:C₂₆H₃₁ClO₃
Molecular Weight:426.983
Hs Code.:

Synonyms:17β-Hydroxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-3-one 17-Benzoate

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Chemical Property of 17β-Hydroxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-3-one 17-Benzoate

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Technology Process of 17β-Hydroxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-3-one 17-Benzoate

There total 4 articles about 17β-Hydroxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-3-one 17-Benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 126792-25-4
6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 17-Benzoate

: 126792-26-5
17β-Hydroxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-3-one 17-Benzoate

Guidance literature:: With jones reagent; In chloroform; acetone; for 0.166667h; Ambient temperature;

Reference yield:

: 6961-53-1
3β-Acetoxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-17-one

: 126792-26-5
17β-Hydroxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-3-one 17-Benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / Lithium terc-butoxyaluminium hydride / tetrahydrofuran / 1 h / Ambient temperature

2: 78 percent / Pyridine / 2 h / Ambient temperature

3: 91 percent / Hydrochloric Acid,conc., Methanol / CHCl₃ / 60 h / 40 °C

4: 85 percent / Jones reagent / CHCl₃; acetone / 0.17 h / Ambient temperature

With pyridine; hydrogenchloride; methanol; jones reagent; lithium tert-butoxyaluminium hydride; In tetrahydrofuran; chloroform; acetone;

Reference yield:

: 126792-23-2
6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate

: 126792-26-5
17β-Hydroxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-3-one 17-Benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / Pyridine / 2 h / Ambient temperature

2: 91 percent / Hydrochloric Acid,conc., Methanol / CHCl₃ / 60 h / 40 °C

3: 85 percent / Jones reagent / CHCl₃; acetone / 0.17 h / Ambient temperature

With pyridine; hydrogenchloride; methanol; jones reagent; In chloroform; acetone;