6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate 17-Benzoate

Base Information

Chemical Name:6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate 17-Benzoate
CAS No.:126792-24-3
Molecular Formula:C₂₈H₃₅ClO₄
Molecular Weight:471.036
Hs Code.:

Synonyms:6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate 17-Benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate 17-Benzoate

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Technology Process of 6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate 17-Benzoate

There total 2 articles about 6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate 17-Benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 126792-23-2
6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate

: 98-88-4
benzoyl chloride

: 126792-24-3
6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate 17-Benzoate

Guidance literature:: With pyridine; for 2h; Ambient temperature;

Reference yield:

: 6961-53-1
3β-Acetoxy-6β-chloro-5-methyl-19-nor-5β-androst-9-en-17-one

: 126792-24-3
6β-Chloro-5-methyl-19-nor-5β-androst-9-ene-3β,17β-diol 3-Acetate 17-Benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Lithium terc-butoxyaluminium hydride / tetrahydrofuran / 1 h / Ambient temperature

2: 78 percent / Pyridine / 2 h / Ambient temperature

With pyridine; lithium tert-butoxyaluminium hydride; In tetrahydrofuran;