N'-hydroxy-1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide

Base Information

Chemical Name:N'-hydroxy-1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide
CAS No.:1571033-09-4
Molecular Formula:C₁₇H₂₁N₃O₅S
Molecular Weight:379.437
Hs Code.:

Synonyms:N'-hydroxy-1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-hydroxy-1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide

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Technology Process of N'-hydroxy-1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide

There total 4 articles about N'-hydroxy-1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.9%

: 1571033-05-0
1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carbonitrile

: 1571033-09-4
N'-hydroxy-1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide

Guidance literature:: With hydroxylamine hydrochloride; triethylamine; In ethanol; at 65 ℃; for 2h;

Reference yield:

: 74597-04-9
m-hydroxybenzyl bromide

: 1571033-09-4
N'-hydroxy-1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / 20 °C

1.2: 4 h / 65 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 70 °C

3.1: hydroxylamine hydrochloride; triethylamine / ethanol / 2 h / 65 °C

With hydroxylamine hydrochloride; potassium carbonate; triethylamine; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 620-24-6
3-Hydroxybenzyl alcohol

: 1571033-09-4
N'-hydroxy-1-(3-(3-(methylsulfonyl)propoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 1.5 h / 0 - 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / 20 °C

2.2: 4 h / 65 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 70 °C

4.1: hydroxylamine hydrochloride; triethylamine / ethanol / 2 h / 65 °C

With carbon tetrabromide; hydroxylamine hydrochloride; potassium carbonate; triethylamine; triphenylphosphine; In ethanol; dichloromethane; N,N-dimethyl-formamide;