Technology Process of C20H24F6IO6P
There total 10 articles about C20H24F6IO6P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
bis(2,2,2-trifluoroethyl)(methyl)phosphonate;
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
at -98 ℃;
C15H18ClO3I;
In
tetrahydrofuran;
at -98 ℃;
for 1.5h;
DOI:10.1016/j.tet.2010.01.083
- Guidance literature:
-
Multi-step reaction with 5 steps
1: TBAF; AcOH / tetrahydrofuran
2: 93 percent / Dess-Martin periodinane / CH2Cl2
3: 93 percent / NaClO2; NaH2PO4 / H2O; 2-methyl-propan-2-ol
4: (CH3)2=C(NMe2)Cl / CH2Cl2
5: tetrahydrofuran / -98 °C
With
sodium chlorite; sodium dihydrogenphosphate; tetrabutyl ammonium fluoride; Dess-Martin periodane; acetic acid;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2007.02.031
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 93 percent / NaClO2; NaH2PO4 / H2O; 2-methyl-propan-2-ol
2: (CH3)2=C(NMe2)Cl / CH2Cl2
3: tetrahydrofuran / -98 °C
With
sodium chlorite; sodium dihydrogenphosphate;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2007.02.031