3-methoxy-2,4,5,6-tetrabromobenzyl bromide

Base Information

• Chemical Name: 3-methoxy-2,4,5,6-tetrabromobenzyl bromide
• CAS No.: 136401-08-6
• Molecular Formula: C₈H₅Br₅O
• Molecular Weight: 516.647
• Mol file: 136401-08-6.mol

Synonyms:3-methoxy-2,4,5,6-tetrabromobenzyl bromide

Chemical Property of 3-methoxy-2,4,5,6-tetrabromobenzyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 3-methoxy-2,4,5,6-tetrabromobenzyl bromide

There total 2 articles about 3-methoxy-2,4,5,6-tetrabromobenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,3,4,6-tetrabromo-5-methoxytoluene (136401-01-9) → 3-methoxy-2,4,5,6-tetrabromobenzyl bromide (136401-08-6)

Guidance literature:

With bromine; In tetrachloromethane; Irradiation;

Reference yield:

Potassium; 2,3,4,6-tetrabromo-5-methyl-phenolate → 3-methoxy-2,4,5,6-tetrabromobenzyl bromide (136401-08-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / butan-2-one / 0.5 h / Heating

2: 90 percent / Br₂ / CCl₄ / Irradiation

With bromine; In tetrachloromethane; butanone;

Reference yield: 83.0%

sodium methylate (124-41-4) + 3-methoxy-2,4,5,6-tetrabromobenzyl bromide (136401-08-6) → 3-methoxy-2,4,5,6-tetrabromobenzyl methyl ether (136401-03-1)

Guidance literature:

In methanol; at 40 - 50 ℃; for 2h;

upstream raw materials:

2,3,4,6-tetrabromo-5-methoxytoluene

Downstream raw materials:

3-methoxy-2,4,5,6-tetrabromobenzyl methyl ether

Refernces