4-<4-(benzyloxy)-3,5-dimethoxyphenyl>-3-(methoxycarbonyl)-3-butenoic acid

Base Information

Chemical Name:4-<4-(benzyloxy)-3,5-dimethoxyphenyl>-3-(methoxycarbonyl)-3-butenoic acid
CAS No.:218960-98-6
Molecular Formula:C₂₁H₂₂O₇
Molecular Weight:386.401
Hs Code.:

Synonyms:4-<4-(benzyloxy)-3,5-dimethoxyphenyl>-3-(methoxycarbonyl)-3-butenoic acid

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Chemical Property of 4-<4-(benzyloxy)-3,5-dimethoxyphenyl>-3-(methoxycarbonyl)-3-butenoic acid

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Technology Process of 4-<4-(benzyloxy)-3,5-dimethoxyphenyl>-3-(methoxycarbonyl)-3-butenoic acid

There total 5 articles about 4-<4-(benzyloxy)-3,5-dimethoxyphenyl>-3-(methoxycarbonyl)-3-butenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 6527-32-8
4-(benzyloxy)-3,5-dimethoxybenzaldehyde

: 106-65-0
Dimethyl succinate

: 218960-98-6
4-<4-(benzyloxy)-3,5-dimethoxyphenyl>-3-(methoxycarbonyl)-3-butenoic acid

Guidance literature:: With sodium methylate; In methanol; for 5.16667h; Heating;
DOI:10.1248/cpb.54.226

Reference yield:

: 100-44-7
benzyl chloride

: 218960-98-6
4-<4-(benzyloxy)-3,5-dimethoxyphenyl>-3-(methoxycarbonyl)-3-butenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / K₂CO₃; NaI / ethanol / 6 h / Heating

2: 69 percent / NaOMe / methanol / 5.17 h / Heating

With sodium methylate; potassium carbonate; sodium iodide; In methanol; ethanol; 2: Stobbe condensation;
DOI:10.1248/cpb.54.226

Reference yield:

: 134-96-3
syringic aldehyde

: 218960-98-6
4-<4-(benzyloxy)-3,5-dimethoxyphenyl>-3-(methoxycarbonyl)-3-butenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / K₂CO₃; NaI / ethanol / 6 h / Heating

2: 69 percent / NaOMe / methanol / 5.17 h / Heating

With sodium methylate; potassium carbonate; sodium iodide; In methanol; ethanol; 2: Stobbe condensation;
DOI:10.1248/cpb.54.226