7-(3,5-dimethylphenyl)-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione

Base Information

Chemical Name:7-(3,5-dimethylphenyl)-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione
CAS No.:634603-22-8
Molecular Formula:C₁₅H₁₆N₂O₂
Molecular Weight:256.304
Hs Code.:

Synonyms:7-(3,5-dimethylphenyl)-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(3,5-dimethylphenyl)-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione

Chemical Property:

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Technology Process of 7-(3,5-dimethylphenyl)-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione

There total 6 articles about 7-(3,5-dimethylphenyl)-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 634603-20-6
7-(3,5-dimethylphenyl)-6,7-dihydro-5H-cyclopenta[e][1,3]oxazine-2,4-dione

: 634603-22-8
7-(3,5-dimethylphenyl)-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione

Guidance literature:: With ammonium hydroxide; for 24h; Heating;
DOI:10.1039/b303658h

Reference yield:

: 39101-54-7
3,5-dimethylphenylacetonitrile

: 634603-22-8
7-(3,5-dimethylphenyl)-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaOEt; diethyl carbonate / Heating

1.2: 61 percent / aq. KOH / ethanol / 0.5 h / Heating

2.1: 93 percent / NaH / dioxane / 2.5 h / Heating

3.1: 55 percent / glacial acetic acid; aq. HCl / 6 h / Heating

4.1: 35 percent / 3 h / 55 - 130 °C

5.1: 90 percent / aq. NH₃ / 24 h / Heating

With hydrogenchloride; ammonium hydroxide; sodium ethanolate; sodium hydride; acetic acid; Diethyl carbonate; In 1,4-dioxane; 2.1: Thorpe-Ziegler reaction;
DOI:10.1039/b303658h

Reference yield:

: 634603-14-8
2-amino-1-cyano-3-(3,5-dimethylphenyl)cyclopent-1-ene

: 634603-22-8
7-(3,5-dimethylphenyl)-1,5,6,7-tetrahydrocyclopentapyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / glacial acetic acid; aq. HCl / 6 h / Heating

2: 35 percent / 3 h / 55 - 130 °C

3: 90 percent / aq. NH₃ / 24 h / Heating

With hydrogenchloride; ammonium hydroxide; acetic acid;
DOI:10.1039/b303658h