ethoxy(di-(1-methylethyl))-2-[4-[(E)-2-(ethoxydimethylsilyl)ethenyl]phenyl]ethenylsilane

Base Information

Chemical Name:ethoxy(di-(1-methylethyl))-2-[4-[(E)-2-(ethoxydimethylsilyl)ethenyl]phenyl]ethenylsilane
CAS No.:915380-21-1
Molecular Formula:C₂₂H₃₈O₂Si₂
Molecular Weight:390.714
Hs Code.:

Synonyms:ethoxy(di-(1-methylethyl))-2-[4-[(E)-2-(ethoxydimethylsilyl)ethenyl]phenyl]ethenylsilane

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Chemical Property of ethoxy(di-(1-methylethyl))-2-[4-[(E)-2-(ethoxydimethylsilyl)ethenyl]phenyl]ethenylsilane

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Technology Process of ethoxy(di-(1-methylethyl))-2-[4-[(E)-2-(ethoxydimethylsilyl)ethenyl]phenyl]ethenylsilane

There total 5 articles about ethoxy(di-(1-methylethyl))-2-[4-[(E)-2-(ethoxydimethylsilyl)ethenyl]phenyl]ethenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 915380-20-0
Ethoxy-diisopropyl-[(E)-2-(4-vinyl-phenyl)-vinyl]-silane

: 5356-83-2
ethoxydimethylvinylsilane

: 915380-21-1
ethoxy(di-(1-methylethyl))-2-[4-[(E)-2-(ethoxydimethylsilyl)ethenyl]phenyl]ethenylsilane

Guidance literature:: Ru(Cl)H(CO)(i-Pr₃P)2; In dichloromethane; at 100 ℃; for 12h;
DOI:10.1021/jo061481t

Reference yield:

: 135005-24-2
[(4-ethenylphenyl)ethynyl]trimethylsilane

: 915380-21-1
ethoxy(di-(1-methylethyl))-2-[4-[(E)-2-(ethoxydimethylsilyl)ethenyl]phenyl]ethenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / KOH / ethanol; tetrahydrofuran; H₂O / 0 - 20 °C

2.1: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane / 2.5 h / 20 °C

2.2: triethylamine / hexane / 1 h

3.1: 58 percent / Ru(Cl)H(CO)(i-Pr₃P)2 / CH₂Cl₂ / 12 h / 100 °C

With potassium hydroxide; Ru(Cl)H(CO)(i-Pr₃P)2; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jo061481t

Reference yield:

: 77123-57-0
4-[(trimethylsilyl)ethynyl]bezaldehyde

: 915380-21-1
ethoxy(di-(1-methylethyl))-2-[4-[(E)-2-(ethoxydimethylsilyl)ethenyl]phenyl]ethenylsilane

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -10 - 20 °C

1.2: 81 percent / tetrahydrofuran; hexane / -20 - 20 °C

2.1: 88 percent / KOH / ethanol; tetrahydrofuran; H₂O / 0 - 20 °C

3.1: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane / 2.5 h / 20 °C

3.2: triethylamine / hexane / 1 h

4.1: 58 percent / Ru(Cl)H(CO)(i-Pr₃P)2 / CH₂Cl₂ / 12 h / 100 °C

With potassium hydroxide; n-butyllithium; Ru(Cl)H(CO)(i-Pr₃P)2; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane; In tetrahydrofuran; ethanol; hexane; dichloromethane; water;
DOI:10.1021/jo061481t