ethyl 2-{[(4-methylphenyl)sulfonyl](5-trimethylsilylprop-2-enyl)amino}pent-4-ynoate

Base Information

Chemical Name:ethyl 2-{[(4-methylphenyl)sulfonyl](5-trimethylsilylprop-2-enyl)amino}pent-4-ynoate
CAS No.:271599-01-0
Molecular Formula:C₂₀H₂₉NO₄SSi
Molecular Weight:407.606
Hs Code.:

Synonyms:ethyl 2-{[(4-methylphenyl)sulfonyl](5-trimethylsilylprop-2-enyl)amino}pent-4-ynoate

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Chemical Property of ethyl 2-{[(4-methylphenyl)sulfonyl](5-trimethylsilylprop-2-enyl)amino}pent-4-ynoate

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Technology Process of ethyl 2-{[(4-methylphenyl)sulfonyl](5-trimethylsilylprop-2-enyl)amino}pent-4-ynoate

There total 3 articles about ethyl 2-{[(4-methylphenyl)sulfonyl](5-trimethylsilylprop-2-enyl)amino}pent-4-ynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 106-95-6
allyl bromide

: 271598-95-9
2-(toluene-4-sulfonylamino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

: 271599-01-0
ethyl 2-{[(4-methylphenyl)sulfonyl](5-trimethylsilylprop-2-enyl)amino}pent-4-ynoate

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 6h;
DOI:10.1002/1099-0690(200109)2001:17<3375::AID-EJOC3375>3.0.CO;2-R

Reference yield:

: 38002-45-8
3-bromo-1-(trimethylsilyl)-1-propyne

: 271599-01-0
ethyl 2-{[(4-methylphenyl)sulfonyl](5-trimethylsilylprop-2-enyl)amino}pent-4-ynoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / K₂CO₃ / acetonitrile

2.1: HCl; H₂O / diethyl ether

2.2: 77 percent / Et₃N / CH₂Cl₂

3.1: 90 percent / K₂CO₃ / acetonitrile

With hydrogenchloride; water; potassium carbonate; In diethyl ether; acetonitrile; 1.1: Alkylation / 2.1: Hydrolysis / 2.2: Tosylation / 3.1: Alkylation;
DOI:10.1039/a910217p

Reference yield:

: 271598-87-9
2-(benzhydrylidene-amino)-5-trimethylsilanyl-pent-4-ynoic acid ethyl ester

: 271599-01-0
ethyl 2-{[(4-methylphenyl)sulfonyl](5-trimethylsilylprop-2-enyl)amino}pent-4-ynoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: HCl; H₂O / diethyl ether

1.2: 77 percent / Et₃N / CH₂Cl₂

2.1: 90 percent / K₂CO₃ / acetonitrile

With hydrogenchloride; water; potassium carbonate; In diethyl ether; acetonitrile; 1.1: Hydrolysis / 1.2: Tosylation / 2.1: Alkylation;
DOI:10.1039/a910217p