Technology Process of C27H40BrNO2Si
There total 4 articles about C27H40BrNO2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole; dmap; tetra-(n-butyl)ammonium iodide;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ja206538k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol; potassium carbonate / 24 h / 60 °C / Inert atmosphere
2: iodine / methanol / 19 h / 23 °C / Inert atmosphere
3: 1H-imidazole; dmap; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
With
1H-imidazole; methanol; dmap; iodine; tetra-(n-butyl)ammonium iodide; potassium carbonate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja206538k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: iodine / methanol / 19 h / 23 °C / Inert atmosphere
2: 1H-imidazole; dmap; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
With
1H-imidazole; dmap; iodine; tetra-(n-butyl)ammonium iodide;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja206538k