ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate

Base Information

Chemical Name:ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate
CAS No.:1520119-91-8
Molecular Formula:C₁₆H₂₆N₂O₄S
Molecular Weight:342.459
Hs Code.:

ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ<sup>6</sup>-sulfanylidene]amino}propanoate

Synonyms:ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate

Suppliers and Price of ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate

There total 3 articles about ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1520119-66-7
N-(2-methoxyphenyl)butane-2-sulfinamide

: 4244-84-2
ethyl β-alaninate hydrochloride

: 1520119-91-8
ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate

Guidance literature:: N-(2-methoxyphenyl)butane-2-sulfinamide; With tert-butylhypochlorite; In tetrachloromethane; at 0 ℃; for 1.5h; Inert atmosphere;

ethyl β-alaninate hydrochloride; With triethylamine; In tetrachloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1055/s-0033-1339760

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 1520119-91-8
ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / toluene / Reflux

2.1: tetrahydrofuran; diethyl ether / 0 °C / Inert atmosphere

3.1: tert-butylhypochlorite / tetrachloromethane / 1.5 h / 0 °C / Inert atmosphere

3.2: 12 h / 20 °C / Inert atmosphere

With thionyl chloride; tert-butylhypochlorite; In tetrahydrofuran; tetrachloromethane; diethyl ether; toluene;
DOI:10.1055/s-0033-1339760

Reference yield:

: 17419-98-6
N?sulfinyl?2?methoxyaniline

: 1520119-91-8
ethyl 3-{[(2-methoxyanilino)oxo-sec-butyl-1λ⁶-sulfanylidene]amino}propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran; diethyl ether / 0 °C / Inert atmosphere

2.1: tert-butylhypochlorite / tetrachloromethane / 1.5 h / 0 °C / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

With tert-butylhypochlorite; In tetrahydrofuran; tetrachloromethane; diethyl ether;
DOI:10.1055/s-0033-1339760