Technology Process of C25H38O6S
There total 5 articles about C25H38O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C29H48O6SSi;
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 25 - 80 ℃;
for 1.16667h;
Molecular sieve;
methyl iodide;
In
tetrahydrofuran;
at 25 ℃;
for 3.5h;
DOI:10.1021/jo200934w
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium tungstate; phenylphosphonate; dihydrogen peroxide / toluene / 2.5 h / 25 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.17 h / 25 - 80 °C / Molecular sieve
2.2: 3.5 h / 25 °C
With
sodium tungstate; phenylphosphonate; tetrabutyl ammonium fluoride; dihydrogen peroxide;
In
tetrahydrofuran; toluene;
DOI:10.1021/jo200934w
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine; carbon tetrabromide; triphenylphosphine / dichloromethane / 0.5 h / 25 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C
2.2: 3.5 h / 0 - 25 °C
3.1: sodium tungstate; phenylphosphonate; dihydrogen peroxide / toluene / 2.5 h / 25 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.17 h / 25 - 80 °C / Molecular sieve
4.2: 3.5 h / 25 °C
With
pyridine; sodium tungstate; carbon tetrabromide; phenylphosphonate; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium hydride; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; toluene; mineral oil;
1.1: Appel reaction;
DOI:10.1021/jo200934w
