(phenethyl)-1-methyldiazomethane

Base Information

Chemical Name:(phenethyl)-1-methyldiazomethane
CAS No.:1609628-66-1
Molecular Formula:C₁₀H₁₂N₂
Molecular Weight:160.219
Hs Code.:

Synonyms:(phenethyl)-1-methyldiazomethane

Suppliers and Price of (phenethyl)-1-methyldiazomethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (phenethyl)-1-methyldiazomethane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (phenethyl)-1-methyldiazomethane

There total 2 articles about (phenethyl)-1-methyldiazomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16602-93-0
4-phenyl-2-butylhydrazone

: 1609628-66-1
(phenethyl)-1-methyldiazomethane

Guidance literature:: With potassium carbonate; silver(l) oxide; In dichloromethane; at -15 ℃; for 0.0283333h; Flow reactor;
DOI:10.1002/anie.201802092

Reference yield:

: 2550-26-7
4-Phenyl-2-butanone

: 1609628-66-1
(phenethyl)-1-methyldiazomethane

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / tetrahydrofuran / 0.17 h / 100 °C / Flow reactor

2: silver(l) oxide; potassium carbonate / dichloromethane / 0.03 h / -15 °C / Flow reactor

With potassium carbonate; hydrazine hydrate; silver(l) oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201802092

Reference yield: 84.0%

: 1609628-66-1
(phenethyl)-1-methyldiazomethane

: 73183-34-3
bis(pinacol)diborane

: 1609628-55-8
2,2'-(4-phenylbutane-2,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: With tetrakis(triphenylphosphine)platinum; In toluene; at 40 ℃; for 6h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tetlet.2014.03.135