8-[3,4-bis(benzyloxy)phenyl]-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

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Chemical Name:8-[3,4-bis(benzyloxy)phenyl]-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
CAS No.:1150586-07-4
Molecular Formula:C₃₃H₃₁BF₂N₂O₂
Molecular Weight:536.429
Hs Code.:

Synonyms:8-[3,4-bis(benzyloxy)phenyl]-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 8-[3,4-bis(benzyloxy)phenyl]-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 8-[3,4-bis(benzyloxy)phenyl]-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 1 articles about 8-[3,4-bis(benzyloxy)phenyl]-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 5447-02-9
3,4-dibenzyloxybenzaldehyde

: 1150586-07-4
8-[3,4-bis(benzyloxy)phenyl]-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: 2,4-dimethyl-1H-pyrrole; 3,4-dibenzyloxybenzaldehyde; With trifluoroacetic acid; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; at 20 ℃; Inert atmosphere;

With boron trifluoride diethyl etherate; triethylamine; In tetrahydrofuran; dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1039/c1cc15061h

Reference yield: 78.0%

: 1150586-07-4
8-[3,4-bis(benzyloxy)phenyl]-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

: 1150586-09-6
8-(3,4-dihydroxyphenyl)-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; chloroform; at 20 ℃; for 24h; under 760.051 Torr;
DOI:10.1039/c1cc15061h