allyl 4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside

Base Information

• Chemical Name: allyl 4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside
• CAS No.: 1241901-04-1
• Molecular Formula: C₂₄H₂₂N₂O₁₀
• Molecular Weight: 498.446

Synonyms:allyl 4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside

Chemical Property of allyl 4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside

Chemical Property:

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Technology Process of allyl 4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside

There total 5 articles about allyl 4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

allyl 4,6-O-benzylidene-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside (1241901-03-0) + 4-Nitrophenyl chloroformate (7693-46-1) → allyl 4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside (1241901-04-1) + N,N'-bis(1-O-allyl-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-glucopyranos-2-yl)urea (1241901-05-2)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 30 ℃; for 0.75h;

DOI:10.1016/j.tet.2012.12.005

Reference yield: 41.0%

allyl 4,6-O-benzylidene-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside (1241901-03-0) + 4-Nitrophenyl chloroformate (7693-46-1) → allyl 4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside (1241901-04-1)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at -30 ℃; for 0.75h;

DOI:10.1016/j.tet.2012.12.005

Reference yield:

allyl 4,6-O-benzylidene-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside (1241901-03-0) → allyl 4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside (1241901-04-1) + N,N'-bis(1-O-allyl-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-α-D-glucopyranos-2-yl)urea (1241901-05-2)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 30 ℃;

DOI:10.1002/ejoc.201000292

upstream raw materials:

allyl 4,6-O-benzylidene-2-deoxy-2-[(p-nitrophenoxy)carbonylamino]-α-D-glucopyranoside

allyl 2-amino-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

4-Nitrophenyl chloroformate

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