[2-{5-(diphenylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]diphenylphosphane

Base Information

Chemical Name:[2-{5-(diphenylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]diphenylphosphane
CAS No.:1300118-04-0
Molecular Formula:C₃₇H₂₆F₂O₂P₂
Molecular Weight:602.557
Hs Code.:

Synonyms:[2-{5-(diphenylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]diphenylphosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2-{5-(diphenylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]diphenylphosphane

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Technology Process of [2-{5-(diphenylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]diphenylphosphane

There total 9 articles about [2-{5-(diphenylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]diphenylphosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1300117-94-5
5-bromo-2,2-difluoro-4-(2-iodophenyl)benzo[d][1,3]dioxole

: 829-85-6
diphenylphosphane

: 1300118-04-0
[2-{5-(diphenylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]diphenylphosphane

Guidance literature:: With potassium acetate; palladium diacetate; In N,N-dimethyl acetamide; at 130 ℃; for 3h; Inert atmosphere;
DOI:10.1002/chem.201101529

Reference yield: 48.0%

: 1300117-97-8
5-iodo-2,2-difluoro-4-(2-iodophenyl)benzo[1,3]dioxole

: 829-85-6
diphenylphosphane

: 1300118-04-0
[2-{5-(diphenylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]diphenylphosphane

Guidance literature:: With potassium acetate; palladium diacetate; In N,N-dimethyl acetamide; at 130 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/chem.201101529

Reference yield: 47.0%

: 1300117-94-5
5-bromo-2,2-difluoro-4-(2-iodophenyl)benzo[d][1,3]dioxole

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1300118-04-0
[2-{5-(diphenylphosphanyl)-2,2-difluorobenzo[d][1,3]dioxol-4-yl}phenyl]diphenylphosphane

Guidance literature:: 5-bromo-2,2-difluoro-4-(2-iodophenyl)benzo[d][1,3]dioxole; With n-butyllithium; In hexane; toluene; at 25 - 100 ℃; Inert atmosphere;

chloro-diphenylphosphine; In hexane; toluene; at 50 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/ejic.201100428