(bicyclo<2.2.1>heptene-5 yle-2)-1 methyl-1 (trimethyl-2,3,6 phenyl)-3 propanol-1

Base Information

• Chemical Name: (bicyclo<2.2.1>heptene-5 yle-2)-1 methyl-1 (trimethyl-2,3,6 phenyl)-3 propanol-1
• CAS No.: 86361-13-9
• Molecular Formula: C₂₀H₂₈O
• Molecular Weight: 284.442
• Mol file: 86361-13-9.mol

Synonyms:(bicyclo<2.2.1>heptene-5 yle-2)-1 methyl-1 (trimethyl-2,3,6 phenyl)-3 propanol-1

Chemical Property of (bicyclo<2.2.1>heptene-5 yle-2)-1 methyl-1 (trimethyl-2,3,6 phenyl)-3 propanol-1

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (bicyclo<2.2.1>heptene-5 yle-2)-1 methyl-1 (trimethyl-2,3,6 phenyl)-3 propanol-1

There total 10 articles about (bicyclo<2.2.1>heptene-5 yle-2)-1 methyl-1 (trimethyl-2,3,6 phenyl)-3 propanol-1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

methyl magnesium iodide (917-64-6) + (bicyclo<2.2.1>heptene-5 yle-2)-1 (trimethyl-2,3,6 phenyl)-3 propanone-1 (86361-11-7,86361-12-8) → (bicyclo<2.2.1>heptene-5 yle-2)-1 methyl-1 (trimethyl-2,3,6 phenyl)-3 propanol-1 (86361-13-9)

Guidance literature:

In diethyl ether; at 0 ℃; for 0.25h;

DOI:10.1016/S0040-4020(01)91839-3

Reference yield:

2-(Bromomethyl)-1,3,4-trimethylbenzene (54757-29-8) → (bicyclo<2.2.1>heptene-5 yle-2)-1 methyl-1 (trimethyl-2,3,6 phenyl)-3 propanol-1 (86361-13-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent

2: 83 percent / diethyl ether / 0.25 h / 0 °C

In diethyl ether;

DOI:10.1016/S0040-4020(01)91839-3

Reference yield:

2-(Bromomethyl)-1,3,4-trimethylbenzene (54757-29-8) → (bicyclo<2.2.1>heptene-5 yle-2)-1 methyl-1 (trimethyl-2,3,6 phenyl)-3 propanol-1, exo (86361-13-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent

2: diethyl ether / 0.25 h / 0 °C

In diethyl ether;

DOI:10.1016/S0040-4020(01)91839-3

upstream raw materials:

methyl magnesium iodide

(bicyclo<2.2.1>heptene-5 yle-2)-1 (trimethyl-2,3,6 phenyl)-3 propanone-1

2-(Bromomethyl)-1,3,4-trimethylbenzene

endo-2-acetyl-5-norbornene

Downstream raw materials:

methyl-3 (trimethyl-2,3,6 phenyl)-5 pentene-1 ol-3