(2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine

Base Information

Chemical Name:(2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine
CAS No.:910541-83-2
Molecular Formula:C₁₉H₂₆N₂O₅
Molecular Weight:362.426
Hs Code.:

Synonyms:(2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine

Suppliers and Price of (2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine

There total 5 articles about (2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910541-82-1
(2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidine

: 910541-83-2
(2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine

Guidance literature:: With acetic acid; at 20 ℃; for 6.5h;
DOI:10.1016/j.tetasy.2006.06.031

Reference yield:

: 910541-80-9
(3aR,6R,6aS)-2-benzyl-6-(1-ethoxyethoxymethyl)tetrahydro-2H-pyrrolo[3,4-d]osoxazol-4(5H)-one

: 910541-83-2
(2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / LiAlH₄ / tetrahydrofuran / 15 h / Heating

2: pyridine / 6 h / 20 °C

3: 710 mg / aq. AcOH / 6.5 h / 20 °C

With pyridine; lithium aluminium tetrahydride; acetic acid; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2006.06.031

Reference yield:

: 162826-84-8
(4R,7R,8S)-2-benzyl-7-hydroxymethyl-1-oxa-2,6-diazabicyclo<3.3.0>octane-5-one

: 910541-83-2
(2R,3S,4S)-3-acetoxy-1-acetyl-4-(benzylacetamidomethyl)-2-hydroxymethylpyrrolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 33 percent / CCl₃CO₂H / CH₂Cl₂ / 23 h / 20 °C

2: 100 percent / LiAlH₄ / tetrahydrofuran / 15 h / Heating

3: pyridine / 6 h / 20 °C

4: 710 mg / aq. AcOH / 6.5 h / 20 °C

With pyridine; lithium aluminium tetrahydride; acetic acid; trichloroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetasy.2006.06.031