(2R,3S,4S)-4-(benzylaminomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidin-3-ol

Base Information

Chemical Name:(2R,3S,4S)-4-(benzylaminomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidin-3-ol
CAS No.:910541-81-0
Molecular Formula:C₁₇H₂₈N₂O₃
Molecular Weight:308.421
Hs Code.:

Synonyms:(2R,3S,4S)-4-(benzylaminomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidin-3-ol

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Chemical Property of (2R,3S,4S)-4-(benzylaminomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidin-3-ol

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Technology Process of (2R,3S,4S)-4-(benzylaminomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidin-3-ol

There total 3 articles about (2R,3S,4S)-4-(benzylaminomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidin-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 910541-80-9
(3aR,6R,6aS)-2-benzyl-6-(1-ethoxyethoxymethyl)tetrahydro-2H-pyrrolo[3,4-d]osoxazol-4(5H)-one

: 910541-81-0
(2R,3S,4S)-4-(benzylaminomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidin-3-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 15h; Heating;
DOI:10.1016/j.tetasy.2006.06.031

Reference yield:

: 160823-80-3
(3aS,3bR,6R,7aR)-2-benzyl-1,2,3a,3b,4,7a-hexahydro-6-phenyl-3,5-dioxa-2,6a-diazacyclopenta pentalen-7-one

: 910541-81-0
(2R,3S,4S)-4-(benzylaminomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidin-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / aq. TFA

2: 33 percent / CCl₃CO₂H / CH₂Cl₂ / 23 h / 20 °C

3: 100 percent / LiAlH₄ / tetrahydrofuran / 15 h / Heating

With lithium aluminium tetrahydride; trifluoroacetic acid; trichloroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetasy.2006.06.031

Reference yield:

: 162826-84-8
(4R,7R,8S)-2-benzyl-7-hydroxymethyl-1-oxa-2,6-diazabicyclo<3.3.0>octane-5-one

: 910541-81-0
(2R,3S,4S)-4-(benzylaminomethyl)-2-(1-ethoxyethoxymethyl)pyrrolidin-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / CCl₃CO₂H / CH₂Cl₂ / 23 h / 20 °C

2: 100 percent / LiAlH₄ / tetrahydrofuran / 15 h / Heating

With lithium aluminium tetrahydride; trichloroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetasy.2006.06.031