bis-(3-vinyl-phenyl)-diazene-N-oxide

Base Information

Chemical Name:bis-(3-vinyl-phenyl)-diazene-N-oxide
CAS No.:71387-67-2
Molecular Formula:C₁₆H₁₄N₂O
Molecular Weight:250.3
Hs Code.:

bis-(3-vinyl-phenyl)-diazene-<i>N</i>-oxide

Synonyms:bis-(3-vinyl-phenyl)-diazene-N-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis-(3-vinyl-phenyl)-diazene-N-oxide

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Technology Process of bis-(3-vinyl-phenyl)-diazene-N-oxide

There total 12 articles about bis-(3-vinyl-phenyl)-diazene-N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 586-39-0,51209-60-0
1-nitro-3-vinyl-benzene

: 15411-43-5
3-vinylaniline

: 71387-67-2
1,2-bis(3-vinylphenyl)diazene oxide

Guidance literature:: With Ru/C; sodium hydroxide; In tetrahydrofuran; ethanol; at 70 ℃; for 24h; Microwave irradiation;
DOI:10.1002/adsc.201200356

Reference yield: 58.0%

: 586-39-0,51209-60-0
1-nitro-3-vinyl-benzene

: 71387-67-2
1,2-bis(3-vinylphenyl)diazene oxide

Guidance literature:: With cerium(IV) oxide; hydrogen; In toluene; at 120 ℃; under 7500.75 Torr; chemoselective reaction;
DOI:10.1016/j.jcat.2018.11.011

Reference yield: 50.0%

: 586-39-0,51209-60-0
1-nitro-3-vinyl-benzene

: 15411-43-5
3-vinylaniline

: 71387-67-2
bis-(3-vinyl-phenyl)-diazene-N-oxide

Guidance literature:: With carbon monoxide; hexasulfonated 2,2'-bis-diphenylphosphinomethylene binaphthyl; palladium dichloride; In water; xylene; at 100 ℃; for 20h; under 90007.2 Torr; Yields of byproduct given;
DOI:10.1016/0040-4039(95)02003-8