C₅₆H₈₆O₁₄

Base Information

Chemical Name:C₅₆H₈₆O₁₄
CAS No.:206255-56-3
Molecular Formula:C₅₆H₈₆O₁₄
Molecular Weight:983.29
Hs Code.:

C<sub>56</sub>H<sub>86</sub>O<sub>14</sub>

Synonyms:C₅₆H₈₆O₁₄

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Chemical Property of C₅₆H₈₆O₁₄

Chemical Property:

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Technology Process of C₅₆H₈₆O₁₄

There total 19 articles about C₅₆H₈₆O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 206255-55-2
C₆₂H₁₀₀O₁₄Si

: 206255-56-3
C₅₆H₈₆O₁₄

Guidance literature:: With pyridine; hydrogen fluoride; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/ja9727631

Reference yield:

: 206255-40-5
6-(tert-Butyl-dimethyl-silanyloxy)-5,5-dimethyl-hexane-2,4-dione

: 206255-56-3
C₅₆H₈₆O₁₄

Guidance literature:: Multi-step reaction with 18 steps

1: 1.) LDA, 3.) p-TsOH

2: NaBH₄, CeCl₃*7H₂O / methanol / -20 °C

3: m-CPBA, NaHCO₃ / CH₂Cl₂

4: DMAP / CH₂Cl₂ / -10 °C

5: Dess-Martin periodinane / Ambient temperature

6: 95 percent / SmI₂ / tetrahydrofuran; methanol / -78 °C

7: 90 percent / LDA / tetrahydrofuran / -78 °C

8: Et₃N / CH₂Cl₂ / -10 °C

9: DBU / tetrahydrofuran / Ambient temperature

10: NaBH₄, CeCl₃*7H₂O / methanol / -20 °C

11: 2,4,6-trichlorobenzoyl chloride, Et₃N / toluene / Ambient temperature

12: HF, pyridine / tetrahydrofuran / Ambient temperature

13: Dess-Martin periodinane / CH₂Cl₂ / Ambient temperature

14: 2.) Ac₂O, DMAP, 3.) OsO₄, NMO, 4.) Pb(OAc)4, Et₃N, 5.) DBU

15: 79 percent / DDQ / CH₂Cl₂; H₂O

16: 95 percent / aq. HF / acetonitrile / Ambient temperature

17: 1.) 2,4,6-trichlorobenzoyl chloride, Et₃N, 2.) DMAP / 1.) toluene, RT, 2.) toluene

18: 81 percent / HF, pyridine / tetrahydrofuran / Ambient temperature

With pyridine; lead(IV) acetate; dmap; sodium tetrahydroborate; osmium(VIII) oxide; N-methyl-2-indolinone; samarium diiodide; cerium(III) chloride; 2,4,6-trichlorobenzoyl chloride; hydrogen fluoride; acetic anhydride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ja9727631

Reference yield:

: 206255-41-6
(3R,4R)-4-Benzyloxy-3-(4-methoxy-benzyloxy)-pentanal

: 206255-56-3
C₅₆H₈₆O₁₄

Guidance literature:: Multi-step reaction with 18 steps

1: 1.) LDA, 3.) p-TsOH

2: NaBH₄, CeCl₃*7H₂O / methanol / -20 °C

3: m-CPBA, NaHCO₃ / CH₂Cl₂

4: DMAP / CH₂Cl₂ / -10 °C

5: Dess-Martin periodinane / Ambient temperature

6: 95 percent / SmI₂ / tetrahydrofuran; methanol / -78 °C

7: 90 percent / LDA / tetrahydrofuran / -78 °C

8: Et₃N / CH₂Cl₂ / -10 °C

9: DBU / tetrahydrofuran / Ambient temperature

10: NaBH₄, CeCl₃*7H₂O / methanol / -20 °C

11: 2,4,6-trichlorobenzoyl chloride, Et₃N / toluene / Ambient temperature

12: HF, pyridine / tetrahydrofuran / Ambient temperature

13: Dess-Martin periodinane / CH₂Cl₂ / Ambient temperature

14: 2.) Ac₂O, DMAP, 3.) OsO₄, NMO, 4.) Pb(OAc)4, Et₃N, 5.) DBU

15: 79 percent / DDQ / CH₂Cl₂; H₂O

16: 95 percent / aq. HF / acetonitrile / Ambient temperature

17: 1.) 2,4,6-trichlorobenzoyl chloride, Et₃N, 2.) DMAP / 1.) toluene, RT, 2.) toluene

18: 81 percent / HF, pyridine / tetrahydrofuran / Ambient temperature

With pyridine; lead(IV) acetate; dmap; sodium tetrahydroborate; osmium(VIII) oxide; N-methyl-2-indolinone; samarium diiodide; cerium(III) chloride; 2,4,6-trichlorobenzoyl chloride; hydrogen fluoride; acetic anhydride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ja9727631