ethyl 2-hydroxy-4-methoxy-3-(3-methylbut-2-en-1-yl)-6-(2-phenylethyl)benzoate

Base Information

Chemical Name:ethyl 2-hydroxy-4-methoxy-3-(3-methylbut-2-en-1-yl)-6-(2-phenylethyl)benzoate
CAS No.:1431610-36-4
Molecular Formula:C₂₃H₂₈O₄
Molecular Weight:368.473
Hs Code.:

Synonyms:ethyl 2-hydroxy-4-methoxy-3-(3-methylbut-2-en-1-yl)-6-(2-phenylethyl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-hydroxy-4-methoxy-3-(3-methylbut-2-en-1-yl)-6-(2-phenylethyl)benzoate

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Technology Process of ethyl 2-hydroxy-4-methoxy-3-(3-methylbut-2-en-1-yl)-6-(2-phenylethyl)benzoate

There total 11 articles about ethyl 2-hydroxy-4-methoxy-3-(3-methylbut-2-en-1-yl)-6-(2-phenylethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: ethyl 4-methoxy-2-[(2-methylbut-3-en-2-yl)oxy]-6-(2-phenylethyl)benzoate

: 1431610-36-4
ethyl 2-hydroxy-4-methoxy-3-(3-methylbut-2-en-1-yl)-6-(2-phenylethyl)benzoate

Guidance literature:: In o-xylene; for 1.16667h; Microwave irradiation; Reflux;
DOI:10.1080/09168451.2019.1618699

Reference yield: 66.0%

: C₂₂H₂₆O₄

: 74-88-4
methyl iodide

: 1431610-36-4
ethyl 2-hydroxy-4-methoxy-3-(3-methylbut-2-en-1-yl)-6-(2-phenylethyl)benzoate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 3h;
DOI:10.1021/acs.joc.0c03043

Reference yield:

: 1431610-33-1
ethyl 2-hydroxy-4-methoxy-6-(2-phenylethyl)-benzoate

: 870-63-3
prenyl bromide

: 1431610-36-4
ethyl 2-hydroxy-4-methoxy-3-(3-methylbut-2-en-1-yl)-6-(2-phenylethyl)benzoate

Guidance literature:: ethyl 2-hydroxy-4-methoxy-6-(2-phenylethyl)-benzoate; With sodium hydride; In toluene; mineral oil; at 20 ℃; for 0.5h; Inert atmosphere;

prenyl bromide; In toluene; mineral oil; at 70 - 75 ℃; for 4h;

With hydrogenchloride; In ethanol; regioselective reaction;
DOI:10.1016/j.tetlet.2013.03.042