20-<(allyloxy)methyl>-4,10-dibenzyl-16,25-diethyl-4,10,16,25-tetraza-1,7,13,19,22-pentaoxacycloheptacosane

Base Information

Chemical Name:20-<(allyloxy)methyl>-4,10-dibenzyl-16,25-diethyl-4,10,16,25-tetraza-1,7,13,19,22-pentaoxacycloheptacosane
CAS No.:118974-40-6
Molecular Formula:C₄₀H₆₆N₄O₆
Molecular Weight:698.987
Hs Code.:

Synonyms:20-<(allyloxy)methyl>-4,10-dibenzyl-16,25-diethyl-4,10,16,25-tetraza-1,7,13,19,22-pentaoxacycloheptacosane

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Chemical Property of 20-<(allyloxy)methyl>-4,10-dibenzyl-16,25-diethyl-4,10,16,25-tetraza-1,7,13,19,22-pentaoxacycloheptacosane

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Technology Process of 20-<(allyloxy)methyl>-4,10-dibenzyl-16,25-diethyl-4,10,16,25-tetraza-1,7,13,19,22-pentaoxacycloheptacosane

There total 4 articles about 20-<(allyloxy)methyl>-4,10-dibenzyl-16,25-diethyl-4,10,16,25-tetraza-1,7,13,19,22-pentaoxacycloheptacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 114719-16-3
4-<(allyloxy)methyl>-1,8-diiodo-3,6-dioxaoctane

: 119004-92-1
[2-(2-{Benzyl-[2-(2-{benzyl-[2-(2-ethylamino-ethoxy)-ethyl]-amino}-ethoxy)-ethyl]-amino}-ethoxy)-ethyl]-ethyl-amine

: 118974-40-6
20-<(allyloxy)methyl>-4,10-dibenzyl-16,25-diethyl-4,10,16,25-tetraza-1,7,13,19,22-pentaoxacycloheptacosane

Guidance literature:: With potassium carbonate; caesium carbonate; potassium iodide; In acetonitrile; for 24h; Heating;
DOI:10.1021/jo00278a016

Reference yield:

: 118974-46-2
N-[2-(2-hydroxyethoxy)ethyl]acetamide

: 118974-40-6
20-<(allyloxy)methyl>-4,10-dibenzyl-16,25-diethyl-4,10,16,25-tetraza-1,7,13,19,22-pentaoxacycloheptacosane

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride

2: anhydrous Na₂CO₃ / toluene / Heating

3: LiAlH₄

4: K₂CO₃, Na₂CO₃, NaI

With lithium aluminium tetrahydride; thionyl chloride; sodium carbonate; potassium carbonate; sodium iodide; In toluene;
DOI:10.1016/0040-4039(88)85282-1

Reference yield:

: 118974-47-3
N-[2-(2-chloroethoxy)ethyl]acetamide. N-[2-(2-hydroxyethoxy)ethyl]acetamide

: 118974-40-6
20-<(allyloxy)methyl>-4,10-dibenzyl-16,25-diethyl-4,10,16,25-tetraza-1,7,13,19,22-pentaoxacycloheptacosane

Guidance literature:: Multi-step reaction with 3 steps

1: anhydrous Na₂CO₃ / toluene / Heating

2: LiAlH₄

3: K₂CO₃, Na₂CO₃, NaI

With lithium aluminium tetrahydride; sodium carbonate; potassium carbonate; sodium iodide; In toluene;
DOI:10.1016/0040-4039(88)85282-1