(S)-cyanomethyl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

Base Information

• Chemical Name: (S)-cyanomethyl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate
• CAS No.: 940932-30-9
• Molecular Formula: C₁₆H₁₉N₅O₄
• Molecular Weight: 345.358

Synonyms:(S)-cyanomethyl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

Chemical Property of (S)-cyanomethyl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

Chemical Property:

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Technology Process of (S)-cyanomethyl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

There total 1 articles about (S)-cyanomethyl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(S)-3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid (33173-55-6) + chloroacetonitrile (107-14-2) → (S)-cyanomethyl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate (940932-30-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; for 12h;

DOI:10.1021/ja2055098

Reference yield: 69.0%

5'-O-dimethoxytrityladenosine (57018-82-3,81352-25-2) + (S)-cyanomethyl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate (940932-30-9) → (S)-(2R,3R,5R)-2-(6-amino-9H-purin-9-yl)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-3-hydroxytetrahydrofuran-4-yl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

Guidance literature:

With tetrabutylammonium acetate; In tetrahydrofuran; for 24h;

Reference yield: 69.0%

5'-O-dimethoxytrityladenosine (57018-82-3,81352-25-2) + (S)-cyanomethyl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate (940932-30-9) → (S)-(2R,3R,4R,5R)-2-(6-amino-9H-purin-9-yl)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4-hydroxytetrahydrofuran-3-yl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate (1333389-13-1)

Guidance literature:

With tetrabutylammonium acetate; In tetrahydrofuran; for 24h;

DOI:10.1021/ja2055098

upstream raw materials:

(S)-3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoic acid

chloroacetonitrile

Downstream raw materials:

(S)-(2R,3R,4R,5R)-2-(6-amino-9H-purin-9-yl)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4-hydroxytetrahydrofuran-3-yl 3-(4-azidophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

(S)-(2R,3R,4R,5R)-2-(6-amino-9H-purin-9-yl)-4-hydroxy-5-(hydroxymethyl)tetrahydrofuran-3-yl 2-amino-3-(4-azidophenyl)propanoate

AzfLysAlaAcm

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