C₂₃H₂₆O₄

Base Information

Chemical Name:C₂₃H₂₆O₄
CAS No.:951024-72-9
Molecular Formula:C₂₃H₂₆O₄
Molecular Weight:366.457
Hs Code.:

C<sub>23</sub>H<sub>26</sub>O<sub>4</sub>

Synonyms:C₂₃H₂₆O₄

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Chemical Property of C₂₃H₂₆O₄

Chemical Property:

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Technology Process of C₂₃H₂₆O₄

There total 8 articles about C₂₃H₂₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 951024-71-8
C₂₆H₂₉O₅N

: 100-39-0
benzyl bromide

: 951024-72-9
C₂₃H₂₆O₄

Guidance literature:: C₂₆H₂₉O₅N; With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 0 - 23 ℃;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 23 ℃; for 2h; Further stages.;
DOI:10.1021/ol701446y

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 951024-72-9
C₂₃H₂₆O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: Br₂ / CH₂Cl₂ / 0.25 h / 0 °C

1.2: Et₃N / CH₂Cl₂ / 0.25 h

1.3: 98 percent / 72 h / 20 °C

2.1: 95 percent / pyridinium p-toluenesulfonate / 1 h / 50 °C / simultaneous removal of volatiles in vacuo

3.1: n-BuLi / hexane / -78 - -50 °C

3.2: 84 percent / hexane; tetrahydrofuran / 0.5 h / -78 °C

4.1: CeCl₃*7H₂O; NaBH₄ / ethanol / 0 °C

5.1: 6.10 g / CuSO₄*5H₂O; H₂O / methanol / 2 h / 50 °C

6.1: MgCl₂; Et₃N; TMSCl / ethyl acetate / 23 °C

6.2: trifluoroacetic acid / methanol

7.1: 82 percent / p-toluenesulfonic acid monohydrate / 23 °C

8.1: aq. H₂O₂; LiOH*H₂O / tetrahydrofuran / 0 - 23 °C

8.2: 91 percent / tetrabutylammonium iodide; K₂CO₃ / dimethylformamide / 2 h / 23 °C

With lithium hydroxide; sodium tetrahydroborate; n-butyllithium; chloro-trimethyl-silane; cerium(III) chloride; water; dihydrogen peroxide; bromine; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; copper(II) sulfate; triethylamine; magnesium chloride; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; ethyl acetate;
DOI:10.1021/ol701446y

Reference yield:

: 33603-90-6
(2Z)-2-bromo-3-phenyl-2-propenal

: 951024-72-9
C₂₃H₂₆O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: 95 percent / pyridinium p-toluenesulfonate / 1 h / 50 °C / simultaneous removal of volatiles in vacuo

2.1: n-BuLi / hexane / -78 - -50 °C

2.2: 84 percent / hexane; tetrahydrofuran / 0.5 h / -78 °C

3.1: CeCl₃*7H₂O; NaBH₄ / ethanol / 0 °C

4.1: 6.10 g / CuSO₄*5H₂O; H₂O / methanol / 2 h / 50 °C

5.1: MgCl₂; Et₃N; TMSCl / ethyl acetate / 23 °C

5.2: trifluoroacetic acid / methanol

6.1: 82 percent / p-toluenesulfonic acid monohydrate / 23 °C

7.1: aq. H₂O₂; LiOH*H₂O / tetrahydrofuran / 0 - 23 °C

7.2: 91 percent / tetrabutylammonium iodide; K₂CO₃ / dimethylformamide / 2 h / 23 °C

With lithium hydroxide; sodium tetrahydroborate; n-butyllithium; chloro-trimethyl-silane; cerium(III) chloride; water; dihydrogen peroxide; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; copper(II) sulfate; triethylamine; magnesium chloride; In tetrahydrofuran; methanol; ethanol; hexane; ethyl acetate;
DOI:10.1021/ol701446y