(+/-)-cis-carbobenzoxycyclobutanecarbonyl chloride

Base Information

Chemical Name:(+/-)-cis-carbobenzoxycyclobutanecarbonyl chloride
CAS No.:82588-20-3
Molecular Formula:C₁₃H₁₃ClO₃
Molecular Weight:252.697
Hs Code.:

Synonyms:(+/-)-cis-carbobenzoxycyclobutanecarbonyl chloride

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Chemical Property of (+/-)-cis-carbobenzoxycyclobutanecarbonyl chloride

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Technology Process of (+/-)-cis-carbobenzoxycyclobutanecarbonyl chloride

There total 3 articles about (+/-)-cis-carbobenzoxycyclobutanecarbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 82588-18-9,92828-74-5
(+/-)-cis-cyclobutane-1,2-dicarboxylic acid monobenzyl ester

: 82588-20-3
(+/-)-cis-carbobenzoxycyclobutanecarbonyl chloride

Guidance literature:: With pyridine; oxalyl dichloride; In benzene; at 0 - 55 ℃; for 24h;
DOI:10.1021/jm00351a016

Reference yield:

: 4462-96-8
cis-1,2-cyclobutane dicarboxylic anhydride

: 82588-20-3
(+/-)-cis-carbobenzoxycyclobutanecarbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / benzene / 4 h / Heating

2: 56 percent / (COCl)2, pyridine / benzene / 24 h / 0 - 55 °C

With pyridine; oxalyl dichloride; In benzene;
DOI:10.1021/jm00351a016

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 82588-20-3
(+/-)-cis-carbobenzoxycyclobutanecarbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / benzene / 4 h / Heating

2: 56 percent / (COCl)2, pyridine / benzene / 24 h / 0 - 55 °C

With pyridine; oxalyl dichloride; In benzene;
DOI:10.1021/jm00351a016