5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole-2,8-dicarbaldehyde

Base Information

Chemical Name:5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole-2,8-dicarbaldehyde
CAS No.:1352420-76-8
Molecular Formula:C₄₄H₄₄N₂O₂
Molecular Weight:632.846
Hs Code.:

Synonyms:5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole-2,8-dicarbaldehyde

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Chemical Property of 5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole-2,8-dicarbaldehyde

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Technology Process of 5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole-2,8-dicarbaldehyde

There total 5 articles about 5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole-2,8-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4885-02-3
Dichloromethyl methyl ether

: 1352420-69-9
5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole

: 1352420-76-8
5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole-2,8-dicarbaldehyde

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -20 - 20 ℃; for 1.25h;
DOI:10.24820/ark.5550190.p010.557

Reference yield: 81.0%

: 1352420-74-6
2,8-dibromo-5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1352420-76-8
5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole-2,8-dicarbaldehyde

Guidance literature:: 2,8-dibromo-5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c1ob06298k

Reference yield:

: 1352420-72-4
5,11-dihexyl-6,12-diphenyl-5,6,11,12-tetrahydroindolo[3,2-b]carbazole

: 1352420-76-8
5,11-dihexyl-6,12-diphenyl-5,11-dihydroindolo[3,2-b]carbazole-2,8-dicarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide; acetic acid / 4 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 - 20 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; acetic acid; In tetrahydrofuran; hexane;
DOI:10.1039/c1ob06298k