N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-aminoacetamide

Base Information

Chemical Name:N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-aminoacetamide
CAS No.:1001407-08-4
Molecular Formula:C₂₀H₂₅FN₂O₉
Molecular Weight:456.425
Hs Code.:

Synonyms:N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-aminoacetamide

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Chemical Property of N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-aminoacetamide

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Technology Process of N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-aminoacetamide

There total 5 articles about N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-aminoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1001407-07-3
N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-(benzyloxycarbonylamino)acetamide

: 1001407-08-4
N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-aminoacetamide

Guidance literature:: With ammonium formate; palladium on activated charcoal; In tetrahydrofuran; ethanol; at 70 ℃; for 0.833333h;
DOI:10.1016/j.bmc.2008.03.038

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1001407-08-4
N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-aminoacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: silver(l) oxide / acetonitrile / 23 h / 20 °C

2: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; ethanol / 23 h / 20 °C

3: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 25 h / 20 °C

4: ammonium formate / tetrahydrofuran; ethanol / 0.83 h / 70 °C

With hydrogen; ammonium formate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; silver(l) oxide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1001407-03-9
4-nitrophenyl 3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranoside

: 1001407-08-4
N-[4-(3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-β-D-glucopyranosyloxy)phenyl]-2-aminoacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; ethanol / 23 h / 20 °C

2: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 25 h / 20 °C

3: ammonium formate / tetrahydrofuran; ethanol / 0.83 h / 70 °C

With hydrogen; ammonium formate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;