methyl {3-amino-2-(2-methoxyphenyl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl}phosphonate

Base Information

• Chemical Name: methyl {3-amino-2-(2-methoxyphenyl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl}phosphonate
• CAS No.: 1392447-74-3
• Molecular Formula: C₁₂H₁₃N₄O₄PS
• Molecular Weight: 340.299

Synonyms:methyl {3-amino-2-(2-methoxyphenyl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl}phosphonate

Chemical Property of methyl {3-amino-2-(2-methoxyphenyl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl}phosphonate

Chemical Property:

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Technology Process of methyl {3-amino-2-(2-methoxyphenyl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl}phosphonate

There total 2 articles about methyl {3-amino-2-(2-methoxyphenyl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl}phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

C13H16N4O4PS(1+)*Cl(1-) → methyl {3-amino-2-(2-methoxyphenyl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl}phosphonate (1392447-74-3)

Guidance literature:

In methanol; isopropyl alcohol;

DOI:10.1016/j.tetlet.2012.05.157

Reference yield:

4-amino-5-(2-methoxyphenyl)-2,3-dihydro-4H-1,2,4-triazole-3-thione (61019-26-9) → methyl {3-amino-2-(2-methoxyphenyl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl}phosphonate (1392447-74-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 20 °C

2: methanol; isopropyl alcohol

In methanol; isopropyl alcohol; acetonitrile;

DOI:10.1016/j.tetlet.2012.05.157

Reference yield: 93.0%

methyl {3-amino-2-(2-methoxyphenyl)-3H-thiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl}phosphonate (1392447-74-3) → hydrogen [3-amino-2-(2-methoxyphenyl)-3Hthiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl]phosphonate (1392447-77-6)

Guidance literature:

With hydrogenchloride; at 70 - 95 ℃;

DOI:10.1134/S1070428013040155

upstream raw materials:

4-amino-5-(2-methoxyphenyl)-2,3-dihydro-4H-1,2,4-triazole-3-thione

Downstream raw materials:

hydrogen [3-amino-2-(2-methoxyphenyl)-3Hthiazolo[3,2-b][1,2,4]triazol-7-ium-6-yl]phosphonate

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