(R)-4-((E)-3-Benzenesulfonylmethoxy-propenyl)-2,2-dimethyl-[1,3]dioxolane

Base Information

Chemical Name:(R)-4-((E)-3-Benzenesulfonylmethoxy-propenyl)-2,2-dimethyl-[1,3]dioxolane
CAS No.:119814-58-3
Molecular Formula:C₁₅H₂₀O₅S
Molecular Weight:312.387
Hs Code.:

Synonyms:(R)-4-((E)-3-Benzenesulfonylmethoxy-propenyl)-2,2-dimethyl-[1,3]dioxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-4-((E)-3-Benzenesulfonylmethoxy-propenyl)-2,2-dimethyl-[1,3]dioxolane

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Technology Process of (R)-4-((E)-3-Benzenesulfonylmethoxy-propenyl)-2,2-dimethyl-[1,3]dioxolane

There total 6 articles about (R)-4-((E)-3-Benzenesulfonylmethoxy-propenyl)-2,2-dimethyl-[1,3]dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 122410-16-6
(R)-2,2-Dimethyl-4-((E)-3-phenylsulfanylmethoxy-propenyl)-[1,3]dioxolane

: 119814-58-3
(R)-4-((E)-3-Benzenesulfonylmethoxy-propenyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4039(00)82180-2

Reference yield:

: 7205-91-6
phenylthiomethyl chloride

: 119814-58-3
(R)-4-((E)-3-Benzenesulfonylmethoxy-propenyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / KH / tetrahydrofuran

2: 92 percent / MCPBA / CH₂Cl₂

With potassium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)82180-2

Reference yield:

: 97776-79-9
4,5-O-isopropylidene-L-arabinose dibenzyl thioacetal

: 119814-58-3
(R)-4-((E)-3-Benzenesulfonylmethoxy-propenyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 5 steps

1: Pb(OAc)4 / CH₂Cl₂

2: 1.) K₂CO₃ / H₂O

3: 95 percent / iBu₂AlH / tetrahydrofuran

4: 57 percent / KH / tetrahydrofuran

5: 92 percent / MCPBA / CH₂Cl₂

With lead(IV) acetate; potassium hydride; diisobutylaluminium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)82180-2