3'-BroMo-3-biphenylboronic Acid

Base Information

• Chemical Name: 3'-BroMo-3-biphenylboronic Acid
• CAS No.: 1048990-21-1
• Molecular Formula: C₁₂H₁₀BBrO₂
• Molecular Weight: 276.925
• Mol file: 1048990-21-1.mol

Synonyms:(3'-bromo-[1,1'-biphenyl]-3-yl)boronic acid

Chemical Property of 3'-BroMo-3-biphenylboronic Acid

Chemical Property:

• Boiling Point: 443.9±47.0 °C(Predicted)
• PKA: 8.25±0.10(Predicted)
• Density: 1.53±0.1 g/cm3(Predicted)
• Storage Temp.: 2-8°C

Purity/Quality:

98.5% ^*data from raw suppliers

(3'-Bromo-[1,1'-biphenyl]-3-yl)boronicacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3'-BroMo-3-biphenylboronic Acid

There total 1 articles about 3'-BroMo-3-biphenylboronic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(3'-Bromo-biphenyl-3-yl)-trimethyl-silane → (3'-bromo-[1,1'-biphenyl]-3-yl)boronic acid (1048990-21-1)

Guidance literature:

With boron tribromide; at 70 ℃;

DOI:10.1021/ja804120r

Reference yield: 88.13%

(3'-bromo-[1,1'-biphenyl]-3-yl)boronic acid (1048990-21-1) + C40H26ClN → C52H34BrN

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 110 ℃; for 5h; Inert atmosphere;

Reference yield: 86.05%

(3'-bromo-[1,1'-biphenyl]-3-yl)boronic acid (1048990-21-1) + C19H15BrS → C31H23BrS

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 90 ℃; for 5h; Inert atmosphere;

Refernces