2-(2-(4-(4-methoxyphenyl)-1H-1,2,3-triazol-1-yl)phenyl)H-imidazo[1,2-a]pyridine

Base Information

• Chemical Name: 2-(2-(4-(4-methoxyphenyl)-1H-1,2,3-triazol-1-yl)phenyl)H-imidazo[1,2-a]pyridine
• CAS No.: 1569809-23-9
• Molecular Formula: C₂₂H₁₇N₅O
• Molecular Weight: 367.41

Synonyms:2-(2-(4-(4-methoxyphenyl)-1H-1,2,3-triazol-1-yl)phenyl)H-imidazo[1,2-a]pyridine

Chemical Property of 2-(2-(4-(4-methoxyphenyl)-1H-1,2,3-triazol-1-yl)phenyl)H-imidazo[1,2-a]pyridine

Chemical Property:

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Technology Process of 2-(2-(4-(4-methoxyphenyl)-1H-1,2,3-triazol-1-yl)phenyl)H-imidazo[1,2-a]pyridine

There total 2 articles about 2-(2-(4-(4-methoxyphenyl)-1H-1,2,3-triazol-1-yl)phenyl)H-imidazo[1,2-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

sodium azide + 2-(2-bromophenyl)imidazo[1,2-α]pyridine (115769-03-4) + 4-methoxyphenylacetylen (768-60-5) → 2-(2-(4-(4-methoxyphenyl)-1H-1,2,3-triazol-1-yl)phenyl)H-imidazo[1,2-a]pyridine (1569809-23-9)

Guidance literature:

With copper(II) choride dihydrate; potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 3h; regioselective reaction;

DOI:10.1055/s-0033-1339927

Reference yield:

2-(2-bromophenyl)imidazo[1,2-α]pyridine (115769-03-4) + 4-methoxyphenylacetylen (768-60-5) → 2-(2-(4-(4-methoxyphenyl)-1H-1,2,3-triazol-1-yl)phenyl)H-imidazo[1,2-a]pyridine (1569809-23-9)

Guidance literature:

With copper(l) iodide; sodium azide; potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 6h;

DOI:10.1021/acs.joc.6b00996

Reference yield:

2-(2-(4-(4-methoxyphenyl)-1H-1,2,3-triazol-1-yl)phenyl)H-imidazo[1,2-a]pyridine (1569809-23-9) → 1-(4-methoxyphenyl)pyrido[2′,1′:2,3]imidazo[4,5-c][1,2,3]-triazolo[1,5-a]quinoline (1450724-93-2)

Guidance literature:

With copper diacetate; palladium diacetate; In acetic acid; at 120 ℃; for 7h;

DOI:10.1021/acs.joc.6b00996

upstream raw materials:

2-(2-bromophenyl)imidazo[1,2-α]pyridine

4-methoxyphenylacetylen

Downstream raw materials:

1-(4-methoxyphenyl)pyrido[2′,1′:2,3]imidazo[4,5-c][1,2,3]-triazolo[1,5-a]quinoline

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