1L-(1,2,4,5/3)-1-C-Benzyloxymethyl-1,3,4-tri-O-benzyl-2-O-methyl-1,2,3,4,5-cyclohexanpentol

Base Information

Chemical Name:1L-(1,2,4,5/3)-1-C-Benzyloxymethyl-1,3,4-tri-O-benzyl-2-O-methyl-1,2,3,4,5-cyclohexanpentol
CAS No.:104976-21-8
Molecular Formula:C₃₆H₄₀O₆
Molecular Weight:568.71
Hs Code.:

Synonyms:1L-(1,2,4,5/3)-1-C-Benzyloxymethyl-1,3,4-tri-O-benzyl-2-O-methyl-1,2,3,4,5-cyclohexanpentol

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Chemical Property of 1L-(1,2,4,5/3)-1-C-Benzyloxymethyl-1,3,4-tri-O-benzyl-2-O-methyl-1,2,3,4,5-cyclohexanpentol

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Technology Process of 1L-(1,2,4,5/3)-1-C-Benzyloxymethyl-1,3,4-tri-O-benzyl-2-O-methyl-1,2,3,4,5-cyclohexanpentol

There total 8 articles about 1L-(1,2,4,5/3)-1-C-Benzyloxymethyl-1,3,4-tri-O-benzyl-2-O-methyl-1,2,3,4,5-cyclohexanpentol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 104976-19-4
1L-(1,2,4/3)-1,3,4-Tri-O-benzyl-1-C-benzyloxymethyl-2-O-methyl-5-O-<(trifluormethyl)sulfonyl>-5-cyclohexen-1,2,3,4,5-pentol

: 104976-21-8
1L-(1,2,4,5/3)-1-C-Benzyloxymethyl-1,3,4-tri-O-benzyl-2-O-methyl-1,2,3,4,5-cyclohexanpentol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield: 76.0%

: 104976-19-4
1L-(1,2,4/3)-1,3,4-Tri-O-benzyl-1-C-benzyloxymethyl-2-O-methyl-5-O-<(trifluormethyl)sulfonyl>-5-cyclohexen-1,2,3,4,5-pentol

: 104976-20-7
1D-(1,2,4/3)-5-C-Benzyloxymethyl-2,3-di-O-benzyl-4-O-methyl-5-cyclohexen-1,2,3,4-tetrol

: 104976-21-8
1L-(1,2,4,5/3)-1-C-Benzyloxymethyl-1,3,4-tri-O-benzyl-2-O-methyl-1,2,3,4,5-cyclohexanpentol

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; at -35 ℃; for 0.5h;

Reference yield:

: 100-39-0
benzyl bromide

: 104976-21-8
1L-(1,2,4,5/3)-1-C-Benzyloxymethyl-1,3,4-tri-O-benzyl-2-O-methyl-1,2,3,4,5-cyclohexanpentol

Guidance literature:: Multi-step reaction with 5 steps

1: NaH / dimethylformamide

2: 95 percent / AcOH (95percent), TFA / 1 h / 60 °C

3: 98 percent / pyridine / CH₂Cl₂ / 1.) 5 min, -40 deg C; 2.) 3 h, room temp.

4: 79 percent / LiN₃ / dimethylformamide / 8 h / 50 °C

5: LiBEt₃H / tetrahydrofuran / 0.5 h / -35 °C

With pyridine; lithium azide; sodium hydride; lithium triethylborohydride; acetic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;