N-methyl-N-phenyl-3-fluorobenzylamine

Base Information

Chemical Name:N-methyl-N-phenyl-3-fluorobenzylamine
CAS No.:16547-14-1
Molecular Formula:C₁₄H₁₄FN
Molecular Weight:215.27
Hs Code.:

Synonyms:N-methyl-N-phenyl-3-fluorobenzylamine

Suppliers and Price of N-methyl-N-phenyl-3-fluorobenzylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-methyl-N-phenyl-3-fluorobenzylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-methyl-N-phenyl-3-fluorobenzylamine

There total 4 articles about N-methyl-N-phenyl-3-fluorobenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 455-38-9
3-fluorobenzoic acid

: 100-61-8
N-methylaniline

: 16547-14-1
N-methyl-N-phenyl-3-fluorobenzylamine

Guidance literature:: With phenylsilane; caesium carbonate; In dibutyl ether; at 120 ℃; for 24h; Schlenk technique;

Reference yield: 82.0%

: 124-38-9,18923-20-1
carbon dioxide

: 58606-65-8
N-[(3-fluorophenyl)methylidene]aniline

: 16547-14-1
N-methyl-N-phenyl-3-fluorobenzylamine

Guidance literature:: With [Ru(1,1,1-tris(diphenylphosphinomethyl)ethane)(trimethylenemethane)]; hydrogen; bis(trifluoromethanesulfonyl)amide; In tetrahydrofuran; at 100 ℃; for 24h; under 15001.5 - 60006 Torr; Autoclave;
DOI:10.1002/anie.201403711

Reference yield:

: 62-53-3
aniline

: 456-48-4
3-Fluorobenzaldehyde

: 16547-14-1
N-methyl-N-phenyl-3-fluorobenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 16 h / Molecular sieve

2: [Ru(1,1,1-tris(diphenylphosphinomethyl)ethane)(trimethylenemethane)]; hydrogen; bis(trifluoromethanesulfonyl)amide / tetrahydrofuran / 24 h / 100 °C / 15001.5 - 60006 Torr / Autoclave

With [Ru(1,1,1-tris(diphenylphosphinomethyl)ethane)(trimethylenemethane)]; hydrogen; bis(trifluoromethanesulfonyl)amide; In tetrahydrofuran; toluene;
DOI:10.1002/anie.201403711