Methyl 5-phenylpent-2-EN-4-ynoate

Base Information

Chemical Name:Methyl 5-phenylpent-2-EN-4-ynoate
CAS No.:27948-26-1
Molecular Formula:C12H10 O2
Molecular Weight:186.21
Hs Code.:2916399090
DSSTox Substance ID:DTXSID70579071
Mol file:27948-26-1.mol

Synonyms:27948-26-1;DTXSID70579071;METHYL 5-PHENYLPENT-2-EN-4-YNOATE

Suppliers and Price of Methyl 5-phenylpent-2-EN-4-ynoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Methyl 5-phenylpent-2-EN-4-ynoate

Chemical Property:

Boiling Point:278.8±32.0 °C(Predicted)
PSA：26.30000
Density:1.10±0.1 g/cm3(Predicted)
LogP:1.76730
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:186.068079557
Heavy Atom Count:14
Complexity:271

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C=CC#CC1=CC=CC=C1

Technology Process of Methyl 5-phenylpent-2-EN-4-ynoate

There total 9 articles about Methyl 5-phenylpent-2-EN-4-ynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 6214-22-8
methyl (Z)-3-bromoacrylate

: 536-74-3
phenylacetylene

: 27948-26-1
(Z)-methyl 5-phenylpent-2-en-4-ynoate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 20 ℃;
DOI:10.1016/S0040-4020(01)00139-9

Reference yield: 90.0%

: 6214-23-9
methyl (2Z)-3-iodoprop-2-enoate

: 536-74-3
phenylacetylene

: 27948-26-1
(Z)-methyl 5-phenylpent-2-en-4-ynoate

Guidance literature:: With potassium carbonate; (triphenylphosphine)(2,2'-bipyridine)copper(I) bromide; In toluene; at 110 ℃; for 8h;
DOI:10.1021/ol049706e DOI:10.1055/s-2005-869893