1,1-ethylenedioxy-8,12aβ-dimethyl-9-phenylthio-1,2,3,4,4a,4b,5,6,10b,11,12,12a-dodecahydro-4aα,4bβ,10bα-7-azachrysene

Base Information

Chemical Name:1,1-ethylenedioxy-8,12aβ-dimethyl-9-phenylthio-1,2,3,4,4a,4b,5,6,10b,11,12,12a-dodecahydro-4aα,4bβ,10bα-7-azachrysene
CAS No.:91292-15-8
Molecular Formula:C₂₇H₃₃NO₂S
Molecular Weight:435.631
Hs Code.:

Synonyms:1,1-ethylenedioxy-8,12aβ-dimethyl-9-phenylthio-1,2,3,4,4a,4b,5,6,10b,11,12,12a-dodecahydro-4aα,4bβ,10bα-7-azachrysene

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Chemical Property of 1,1-ethylenedioxy-8,12aβ-dimethyl-9-phenylthio-1,2,3,4,4a,4b,5,6,10b,11,12,12a-dodecahydro-4aα,4bβ,10bα-7-azachrysene

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Technology Process of 1,1-ethylenedioxy-8,12aβ-dimethyl-9-phenylthio-1,2,3,4,4a,4b,5,6,10b,11,12,12a-dodecahydro-4aα,4bβ,10bα-7-azachrysene

There total 1 articles about 1,1-ethylenedioxy-8,12aβ-dimethyl-9-phenylthio-1,2,3,4,4a,4b,5,6,10b,11,12,12a-dodecahydro-4aα,4bβ,10bα-7-azachrysene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13522-48-0
3-(phenylthio)-but-3-en-2-one

: 99745-29-6
(4aS,4bS,8aS)-(+)-8,8-(Ethylendioxy)-4,4a,4b,5,6,7,8,8a,9,10-decahydro-8a-methyl-2(3H)-phenanthrenon

: 91292-15-8
1,1-ethylenedioxy-8,12aβ-dimethyl-9-phenylthio-1,2,3,4,4a,4b,5,6,10b,11,12,12a-dodecahydro-4aα,4bβ,10bα-7-azachrysene

: 91292-10-3
1,1-ethylenedioxy-6a-hydroxy-12aβ-methyl-9-phenylthio-4aα,4bβ,10bα-perhydrochrysen-8-one

Guidance literature:: With ammonia; lithium; tert-butyl alcohol; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 30 min, 2.) THF, -78 deg C, 1 h; room temperature, 3 h; 40 deg C, 2,5 h;