carbonic acid 2-tert-butoxycarbonyloxy-4-(1-phenyl-1H-tetrazole-5-sulfonylmethyl)-phenyl ester tert-butyl ester

Base Information

• Chemical Name: carbonic acid 2-tert-butoxycarbonyloxy-4-(1-phenyl-1H-tetrazole-5-sulfonylmethyl)-phenyl ester tert-butyl ester
• CAS No.: 959588-79-5
• Molecular Formula: C₂₄H₂₈N₄O₈S
• Molecular Weight: 532.574

Synonyms:carbonic acid 2-tert-butoxycarbonyloxy-4-(1-phenyl-1H-tetrazole-5-sulfonylmethyl)-phenyl ester tert-butyl ester

Chemical Property of carbonic acid 2-tert-butoxycarbonyloxy-4-(1-phenyl-1H-tetrazole-5-sulfonylmethyl)-phenyl ester tert-butyl ester

Chemical Property:

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Technology Process of carbonic acid 2-tert-butoxycarbonyloxy-4-(1-phenyl-1H-tetrazole-5-sulfonylmethyl)-phenyl ester tert-butyl ester

There total 1 articles about carbonic acid 2-tert-butoxycarbonyloxy-4-(1-phenyl-1H-tetrazole-5-sulfonylmethyl)-phenyl ester tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C24H28N4O6S (1036244-45-7) → carbonic acid 2-tert-butoxycarbonyloxy-4-(1-phenyl-1H-tetrazole-5-sulfonylmethyl)-phenyl ester tert-butyl ester (959588-79-5)

Guidance literature:

With ammonium molybdate(VI) tetrahydrate; dihydrogen peroxide; In ethanol; at 23 ℃; for 14h;

DOI:10.1016/j.tet.2008.02.108

Reference yield: 80.0%

[4-bromo-3,5-bis-(1,1-dimethyl-allyloxy)]benzaldehyde (959588-81-9) + carbonic acid 2-tert-butoxycarbonyloxy-4-(1-phenyl-1H-tetrazole-5-sulfonylmethyl)-phenyl ester tert-butyl ester (959588-79-5) → (E)-carbonic acid 4-{2-[4-bromo-3,5-bis(1,1-dimethylallyloxy)phenyl]-vinyl}-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester (959588-78-4)

Guidance literature:

With potassium hexamethylsilazane; In tetrahydrofuran; at -78 - 23 ℃; for 3h;

DOI:10.1002/anie.200702363

upstream raw materials:

C₂₄H₂₈N₄O₆S

Downstream raw materials:

(E)-carbonic acid 4-{2-[4-bromo-3,5-bis(1,1-dimethylallyloxy)phenyl]-vinyl}-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

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