N′-((4-methoxyphenyl)(phenyl)methylene)-4-methylbenzenesulfonohydrazide

Base Information

• Chemical Name: N′-((4-methoxyphenyl)(phenyl)methylene)-4-methylbenzenesulfonohydrazide
• CAS No.: 32117-53-6
• Molecular Formula: C₂₁H₂₀N₂O₃S
• Molecular Weight: 380.467

Synonyms:N′-((4-methoxyphenyl)(phenyl)methylene)-4-methylbenzenesulfonohydrazide

Chemical Property of N′-((4-methoxyphenyl)(phenyl)methylene)-4-methylbenzenesulfonohydrazide

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Technology Process of N′-((4-methoxyphenyl)(phenyl)methylene)-4-methylbenzenesulfonohydrazide

There total 1 articles about N′-((4-methoxyphenyl)(phenyl)methylene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-Methoxybenzophenone (611-94-9) + toluene-4-sulfonic acid hydrazide (1576-35-8) → N′-((4-methoxyphenyl)(phenyl)methylene)-4-methylbenzenesulfonohydrazide (32117-53-6)

Guidance literature:

In methanol; at 60 ℃; for 0.0833333 - 1h;

DOI:10.1021/acs.joc.8b02623

Reference yield: 85.0%

trimethylamine-borane (75-22-9) + N′-((4-methoxyphenyl)(phenyl)methylene)-4-methylbenzenesulfonohydrazide (32117-53-6) → trimethylamine-(4-methoxylphenyl)(phenyl)methylborane

Guidance literature:

With rhodium(II) pivalate; lithium tert-butoxide; In 1,2-dichloro-ethane; at 55 ℃; for 4h; Inert atmosphere; Schlenk technique;

DOI:10.1021/jacs.8b05946

Reference yield: 84.0%

N′-((4-methoxyphenyl)(phenyl)methylene)-4-methylbenzenesulfonohydrazide (32117-53-6) → p-methoxyphenyl(phenyl)methyl p-tolyl sulfone

Guidance literature:

With copper(l) iodide; potassium carbonate; In 1,4-dioxane; at 110 ℃; for 2h;

DOI:10.1021/ol101955x

upstream raw materials:

4-Methoxybenzophenone

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

1-(4-methoxyphenyl)-1,2,2-triphenylcyclopropane

2-((4’-methoxyphenyl)(phenyl)methyl)benzo[d]oxazole

1-(tert-butyl)-4-((4-methoxyphenyl)(phenyl)methyl)benzene

p-benzylanizole

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