N,N-diethyl-N'-[4-(4-nitro-phenylsulfanyl)-phenyl]-ethylenediamine

Base Information

• Chemical Name: N,N-diethyl-N'-[4-(4-nitro-phenylsulfanyl)-phenyl]-ethylenediamine
• CAS No.: 767357-13-1
• Molecular Formula: C₁₈H₂₃N₃O₂S
• Molecular Weight: 345.466
• Mol file: 767357-13-1.mol

Synonyms:N,N-diethyl-N'-[4-(4-nitro-phenylsulfanyl)-phenyl]-ethylenediamine

Chemical Property of N,N-diethyl-N'-[4-(4-nitro-phenylsulfanyl)-phenyl]-ethylenediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-diethyl-N'-[4-(4-nitro-phenylsulfanyl)-phenyl]-ethylenediamine

There total 1 articles about N,N-diethyl-N'-[4-(4-nitro-phenylsulfanyl)-phenyl]-ethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-amino-4'-nitrodiphenyl sulfide (101-59-7) + 2-(diethylamino)ethyl chloride (100-35-6) → N,N-diethyl-N'-[4-(4-nitro-phenylsulfanyl)-phenyl]-ethylenediamine (767357-13-1)

Guidance literature:

With nitrobenzene; at 120 - 130 ℃;

DOI:10.1021/ja01218a507

Reference yield:

N,N-diethyl-N'-[4-(4-nitro-phenylsulfanyl)-phenyl]-ethylenediamine (767357-13-1) → N,N-diethyl-N'-[4-(4-amino-phenylsulfanyl)-phenyl]-ethylenediamine

Guidance literature:

With ethanol; iron; acetic acid;

DOI:10.1021/ja01218a507

Reference yield:

N,N-diethyl-N'-[4-(4-nitro-phenylsulfanyl)-phenyl]-ethylenediamine (767357-13-1) → N,N-diethyl-N'-[4-(4-nitro-benzenesulfinyl)-phenyl]-ethylenediamine

Guidance literature:

With dihydrogen peroxide; acetic acid; zuletzt unter Erwaermen;

DOI:10.1021/ja01218a507

upstream raw materials:

4-amino-4'-nitrodiphenyl sulfide

2-(diethylamino)ethyl chloride