2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl6-O-[2,3,4,6-tetra-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl) methyl-β-D-glucopyranoside

Base Information

Chemical Name:2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl6-O-[2,3,4,6-tetra-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl) methyl-β-D-glucopyranoside
CAS No.:1600528-65-1
Molecular Formula:C₉₀H₁₀₂O₁₃Si₂
Molecular Weight:1447.96
Hs Code.:

2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl6-O-[2,3,4,6-tetra-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl) methyl-β-D-glucopyranoside

Synonyms:2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl6-O-[2,3,4,6-tetra-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl) methyl-β-D-glucopyranoside

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Chemical Property of 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl6-O-[2,3,4,6-tetra-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl) methyl-β-D-glucopyranoside

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Technology Process of 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl6-O-[2,3,4,6-tetra-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl) methyl-β-D-glucopyranoside

There total 1 articles about 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl6-O-[2,3,4,6-tetra-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl) methyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1600528-62-8
2,3,4,6-tetra-O-(2-naphthyl)methyl-D-glucopyranosyl-β-(1→6)-3-O-allyl-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside

: 246872-15-1
2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethanol

: 1600528-65-1
2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl6-O-[2,3,4,6-tetra-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl) methyl-β-D-glucopyranoside

Guidance literature:: 2,3,4,6-tetra-O-(2-naphthyl)methyl-D-glucopyranosyl-β-(1→6)-3-O-allyl-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside; 2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethanol; at -60 ℃; for 0.666667h; Inert atmosphere; Molecular sieve;

With N-iodo-succinimide; TMSOTf; at -40 ℃; for 18h; Molecular sieve; Inert atmosphere;
DOI:10.1039/c3ob42503g

Reference yield: 60.0%

: 1600528-65-1
2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl6-O-[2,3,4,6-tetra-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl) methyl-β-D-glucopyranoside

: 203118-32-5
(E)-3-(3,4-bis((tert-butyldimethylsilyl)oxy)phenyl)acrylic acid

: 1600528-67-3
2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]-ethyl4-O-[3,4-bis-(O-tert-butyldimethylsilyl)caffeoyl]-6-O-[2,3,4,6-tetra-O-(2-naphthyl)methyl-β-D-glucopyranosyl]-3-O-allyl-2-O-(2-naphthyl)methyl-β-D-glucopyranoside

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1039/c3ob42503g