4-(ALLYLOXY)BENZOIC ACID

Base Information

• Chemical Name: 4-(ALLYLOXY)BENZOIC ACID
• CAS No.: 27914-60-9
• Molecular Formula: C10H10 O3
• Molecular Weight: 178.188
• Hs Code.: 29189990
• Mol file: 27914-60-9.mol

Synonyms:Benzoicacid, 4-(2-propenyloxy)- (9CI); Benzoic acid, p-(allyloxy)- (6CI,8CI);4-(2-Propenyloxy)benzoic acid; 4-Allyloxybenzoic acid; p-Allyloxybenzoic acid

Chemical Property of 4-(ALLYLOXY)BENZOIC ACID

Chemical Property:

• Melting Point: 163-166°C
• PSA: 46.53000
• LogP: 1.94960
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

4-(Allyloxy)benzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(ALLYLOXY)BENZOIC ACID

There total 21 articles about 4-(ALLYLOXY)BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

allyl (4-allyloxy)benzoate (26595-60-8) → 4-allyloxybenzoic acid (27914-60-9)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In benzene; at 65 - 70 ℃; for 3h;

DOI:10.1055/S-2008-1072727

Reference yield: 98.0%

4-(2-propenyloxy)benzaldehyde (40663-68-1) → 4-allyloxybenzoic acid (27914-60-9)

Guidance literature:

With 2-methyl-but-2-ene; polymer-supported chlorite; acetic acid; In tert-butyl alcohol; at 25 ℃;

DOI:10.1055/s-2001-17448

Reference yield: 95.0%

allyl bromide (106-95-6) + 2'-(trimethylsilyl)ethyl-4-hydroxybenzoate (176700-52-0) → 4-allyloxybenzoic acid (27914-60-9)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/S0040-4039(01)01859-7

upstream raw materials:

ethyl 4-(n-prop-2'-enyloxy)benzoate

allyl bromide

4-hydroxy-benzoic acid

4-(2-propenyloxy)benzaldehyde

Downstream raw materials:

4-(4-allyloxyphenylcarboxy)benzaldehyde

4-hydroxy-benzoic acid

4-fluorophenyl 4-allyloxybenzoate

C₂₄H₂₀O₆

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