3-bromobenzaldehyde trisylhydrazone

Base Information

• Chemical Name: 3-bromobenzaldehyde trisylhydrazone
• CAS No.: 175439-87-9
• Molecular Formula: C₂₂H₂₉BrN₂O₂S
• Molecular Weight: 465.454
• Mol file: 175439-87-9.mol

Synonyms:3-bromobenzaldehyde trisylhydrazone

Chemical Property of 3-bromobenzaldehyde trisylhydrazone

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3-bromobenzaldehyde trisylhydrazone

There total 1 articles about 3-bromobenzaldehyde trisylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-bromobenzoic aldehyde (3132-99-8) + trisylhydrazine (39085-59-1) → 3-bromobenzaldehyde trisylhydrazone (175439-87-9)

Guidance literature:

In methanol; for 1h; Ambient temperature;

DOI:10.1021/jo962089q

Reference yield: 96.0%

tributyl borane (122-56-5) + 3-bromobenzaldehyde trisylhydrazone (175439-87-9) → 1-bromo-3-pentyl-benzene

Guidance literature:

With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; methanol; for 0.5h; Ambient temperature;

DOI:10.1021/jo962089q

Reference yield:

tributyl borane (122-56-5) + 3-bromobenzaldehyde trisylhydrazone (175439-87-9) → 1-(3-bromophenyl)-1-pentanol (158918-39-9)

Guidance literature:

With peracetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; Yield given. Multistep reaction; 1.) THF, room temperature, 1 h;

DOI:10.1080/00397919608003704

upstream raw materials:

m-bromobenzoic aldehyde

trisylhydrazine

Downstream raw materials:

1-(3-bromophenyl)-1-pentanol