C₂₅H₃₅N₃O₅S₂

Base Information

Chemical Name:C₂₅H₃₅N₃O₅S₂
CAS No.:1290128-18-5
Molecular Formula:C₂₅H₃₅N₃O₅S₂
Molecular Weight:521.702
Hs Code.:

C<sub>25</sub>H<sub>35</sub>N<sub>3</sub>O<sub>5</sub>S<sub>2</sub>

Synonyms:C₂₅H₃₅N₃O₅S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₅N₃O₅S₂

Chemical Property:

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Technology Process of C₂₅H₃₅N₃O₅S₂

There total 10 articles about C₂₅H₃₅N₃O₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 542-69-8
1-iodo-butane

: 1290128-03-8
tert-butyl[3-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-6-(methylthio)pyrazolo[5,1-b][1,3]thiazol-7-yl]carbamate

: 1290128-18-5
C₂₅H₃₅N₃O₅S₂

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

Reference yield:

: 1190854-45-5
1-[2,6-dimethoxy-4-(methoxymethyl)phenyl]ethanone

: 1290128-18-5
C₂₅H₃₅N₃O₅S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: triethylamine; t-butyldimethylsiyl triflate / tetrahydrofuran / Cooling with ice

1.2: 1.5 h

1.3: Cooling with ice

2.1: sodium sulfide / N,N-dimethyl-formamide / 2 h / 90 °C

2.2: 2 h / 20 °C

3.1: hydrogenchloride / isopropyl alcohol; water / 20 h / Reflux

4.1: sodium hydroxide; water / ethanol / 2 h / Reflux

4.2: Cooling with ice

5.1: hydrogenchloride / 1,4-dioxane; water / 13 h / Reflux

6.1: L-proline; sodium hydroxide; copper(l) iodide / dimethyl sulfoxide / 3 h / 140 °C / Microwave irradiation

7.1: lithium aluminium tetrahydride; titanium tetrachloride / tetrahydrofuran / 2 h / -78 - 50 °C

7.2: Cooling with ice

8.1: hydrogenchloride; sodium nitrite / water / 3 h / 0 - 20 °C

8.2: Cooling with ice

8.3: 1 h / 20 °C

9.1: triethylamine / dichloromethane / 15 h / 20 °C

10.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 20 °C

With hydrogenchloride; sodium sulfide; copper(l) iodide; lithium aluminium tetrahydride; t-butyldimethylsiyl triflate; water; titanium tetrachloride; sodium hydride; triethylamine; L-proline; sodium hydroxide; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 1290127-98-8
ethyl 6-bromo-3-[2,6-dimethoxy-4-(methoxymethyl)phenyl]pyrazolo[5,1-b][1,3]thiazole-7-carboxylate

: 1290128-18-5
C₂₅H₃₅N₃O₅S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide; water / ethanol / 2 h / Reflux

1.2: Cooling with ice

2.1: hydrogenchloride / 1,4-dioxane; water / 13 h / Reflux

3.1: L-proline; sodium hydroxide; copper(l) iodide / dimethyl sulfoxide / 3 h / 140 °C / Microwave irradiation

4.1: lithium aluminium tetrahydride; titanium tetrachloride / tetrahydrofuran / 2 h / -78 - 50 °C

4.2: Cooling with ice

5.1: hydrogenchloride; sodium nitrite / water / 3 h / 0 - 20 °C

5.2: Cooling with ice

5.3: 1 h / 20 °C

6.1: triethylamine / dichloromethane / 15 h / 20 °C

7.1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 20 °C

With hydrogenchloride; copper(l) iodide; lithium aluminium tetrahydride; water; titanium tetrachloride; sodium hydride; triethylamine; L-proline; sodium hydroxide; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;