6-oxo-6H-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide

Base Information

Chemical Name:6-oxo-6H-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide
CAS No.:375388-65-1
Molecular Formula:C₂₃H₂₃NO₃Si
Molecular Weight:389.526
Hs Code.:

6-oxo-6<i>H</i>-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide

Synonyms:6-oxo-6H-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide

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Chemical Property of 6-oxo-6H-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide

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Technology Process of 6-oxo-6H-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide

There total 4 articles about 6-oxo-6H-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75611-67-5
Pyran-2-one-6-carbonyl chloride

: 375388-63-9
benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amine

: 375388-65-1
6-oxo-6H-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1055/s-2001-16784

Reference yield:

: 2632-83-9
chloro(chloromethyl)methyl(phenyl)silane

: 375388-65-1
6-oxo-6H-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / CuCN / tetrahydrofuran / 20 °C

2: 67 percent / Et₃N / 2 h / 100 °C

3: 80 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With triethylamine; CuCN; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2001-16784

Reference yield:

: phenylmagnesium bromide

: 375388-65-1
6-oxo-6H-pyran-2-carboxylic acid benzyl-[(methyl-phenyl-vinyl-silanyl)-methyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / diethyl ether / Heating

2: 63 percent / CuCN / tetrahydrofuran / 20 °C

3: 67 percent / Et₃N / 2 h / 100 °C

4: 80 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With triethylamine; CuCN; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1055/s-2001-16784