4-METHOXYTOLUENE-D7

Base Information

Chemical Name:4-METHOXYTOLUENE-D7
CAS No.:1036431-36-3
Molecular Formula:C₈H₁₀O
Molecular Weight:129.111
Hs Code.:
Mol file:1036431-36-3.mol

Synonyms:C₈⁽²⁾H₇H₃O

Suppliers and Price of 4-METHOXYTOLUENE-D7

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Medical Isotopes, Inc.
4-Methoxy(toluene-d7)
1 g
$ 1450.00

Medical Isotopes, Inc.
4-Methoxy(toluene-d7)
0.5 g
$ 805.00

Total 6 raw suppliers

Chemical Property of 4-METHOXYTOLUENE-D7

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

4-Methoxy(toluene-d7) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 4-Methoxy(toluene-d7) (CAS# 1036431-36-3) is a useful isotopically labeled research compound.

Technology Process of 4-METHOXYTOLUENE-D7

There total 1 articles about 4-METHOXYTOLUENE-D7 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 202325-52-8
[²H₈]-4-methylphenol

: 74-88-4
methyl iodide

: 1036431-36-3,350818-57-4
C₈⁽²⁾H₇H₃O

Guidance literature:: With potassium carbonate; In acetonitrile;
DOI:10.1002/jlcr.1404

Reference yield:

: 1036431-36-3,350818-57-4
C₈⁽²⁾H₇H₃O

: C₈⁽²⁾H₆H₃OBr

Guidance literature:: With N-Bromosuccinimide; In tetrachloromethane; Irradiation;
DOI:10.1002/jlcr.1404

Reference yield:

: 1036431-36-3,350818-57-4
C₈⁽²⁾H₇H₃O

: 1036431-44-3
C₁₆⁽²⁾H₈H₁₀O₂S⁽¹³⁾C

Guidance literature:: Multi-step reaction with 10 steps

1: N-bromosuccinimide / CCl₄ / Irradiation

2: 79 percent / 18-crown-6 / acetonitrile / 4 h / Heating

3: 80 percent / Na; deuterium oxide / 3 h / Heating

4: 91 percent / deuterium bromide / 0.08 h / 150 °C / microwave irradiation

5: 91 percent / DIEA / acetonitrile / microwave irradiation

6: lithium aluminum deuteride / diethyl ether

7: deuterium oxide; deuterium chloride

8: 91 percent / EtOD; NaOD

9: 94 percent / Et₃N / CH₂Cl₂

10: 71 percent / cesium carbonate / dimethylformamide

With N-Bromosuccinimide; lithium aluminium deuteride; deuteriated sodium hydroxide; 18-crown-6 ether; ethyl [2]alcohol; water-d2; sodium; hydrogen chloride; deuterium bromide; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrachloromethane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/jlcr.1404