(1S,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol

Base Information

• Chemical Name: (1S,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol
• CAS No.: 84066-33-1
• Molecular Formula: C₂₄H₃₂O₅
• Molecular Weight: 400.515

Synonyms:(1S,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol

Chemical Property of (1S,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol

Chemical Property:

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Technology Process of (1S,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol

There total 3 articles about (1S,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3-Dimethoxycyclobutanon (38425-58-0) + (4S,6S)-4-Benzyloxymethoxy-6-isopropenyl-3-methyl-cyclohex-2-enone (84066-30-8) → (1R,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol (84066-33-1) + (1S,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol (84066-33-1)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/ja00341a055

Reference yield:

3,3-Dimethoxycyclobutanon (38425-58-0) + (4S,6S)-4-Benzyloxymethoxy-6-isopropenyl-3-methyl-cyclohex-2-enone (84066-30-8) → (1R,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol (84066-33-1) + (1S,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol (84066-33-1)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/ja00341a055

Reference yield:

3-Ethoxy-3-methoxy-cyclobutanone + (4S,6S)-4-Benzyloxymethoxy-6-isopropenyl-3-methyl-cyclohex-2-enone (84066-30-8) → (1S,4S,6S)-4-Benzyloxymethoxy-1-(3-ethoxy-3-methoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol + (1R,4S,6S)-4-Benzyloxymethoxy-1-(3,3-dimethoxy-cyclobut-1-enyl)-6-isopropenyl-3-methyl-cyclohex-2-enol (84066-33-1)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/ja00341a055

upstream raw materials:

3,3-Dimethoxycyclobutanon

(4S,6S)-4-Benzyloxymethoxy-6-isopropenyl-3-methyl-cyclohex-2-enone

Downstream raw materials:

(3Z,7E)-(1R,5S,10S)-5-Benzyloxymethoxy-11,11-dimethoxy-4,8-dimethyl-bicyclo[8.2.0]dodeca-3,7-dien-2-one

(3Z,7E)-(1S,5S,10S)-5-Benzyloxymethoxy-11,11-dimethoxy-4,8-dimethyl-bicyclo[8.2.0]dodeca-3,7-dien-2-one

germacranolide eucannabinolide

(5Z,9E)-(3aS,7S,11aS)-7-Benzyloxymethoxy-6,10-dimethyl-3,3a,7,8,11,11a-hexahydro-cyclodeca[b]furan-2,4-dione

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