Chloro[2-(dimethylamino)ethyl]boranyl

Base Information

• Chemical Name: Chloro[2-(dimethylamino)ethyl]boranyl
• CAS No.: 1739-26-0
• Molecular Formula: C₄H₁₁BClN
• Molecular Weight: 119.402
• DSSTox Substance ID: DTXSID60701304
• Wikidata: Q82632910
• Mol file: 1739-26-0.mol

Synonyms:DTXSID60701304;Chloro[2-(dimethylamino)ethyl]boranyl

Chemical Property of Chloro[2-(dimethylamino)ethyl]boranyl

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 118.0594822
• Heavy Atom Count: 7
• Complexity: 40.7

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: [B](CCN(C)C)Cl

Technology Process of Chloro[2-(dimethylamino)ethyl]boranyl

There total 7 articles about Chloro[2-(dimethylamino)ethyl]boranyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

bis(dimethylamino)-ethylborane (7318-89-0) + phenylborondichloride (873-51-8) → (dimethylamino)chloroethylborane (1739-26-0)

Guidance literature:

Reference yield: 64.0%

phenylborondichloride (873-51-8) → (dimethylamino)chloroethylborane (1739-26-0)

Guidance literature:

With dimethyl amine; triethylamine; In pentane; -80°C;

Reference yield: 48.0%

ethyl-dichloro-borane (1739-53-3) + 1,1,3,3-tetrakis(dimethylamino)-2-dimethylamino-triboran(5) (26459-62-1) → (dimethylamino)chloroethylborane (1739-26-0) + 1,3-dichloro-1,2,3-tris(dimethylamino)triborane(5) (133911-60-1)

Guidance literature:

In benzene; anhydrous and oxygen-free condns., dropwise addn. of EtBCl2 in benzene to a stirred soln. of B-compd. in benzene, stirred for 14 h; removal of volatile compds. in vac. (EtB(Cl)NMe2), fractional distn.; elem. anal.;

upstream raw materials:

bis(dimethylamino)-ethylborane

ethyl-dichloro-borane

1,2-diethyl-1,2-bis(dimethylamino) diborane

dimethyl amine

Downstream raw materials:

1,2-diethyl-1,2-bis(dimethylamino) diborane

But-1-en-3-yl(dimethylamino)aethylboran

But-2-en-1-yl-(dimethylamino)-aethylboran

Refernces